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The Icing Research Tunnel at NASA Glenn follows the recommended practice for calibration outlined in SAE’s ARP5905. The calibration team has followed the schedule of a full calibration every five years with a check calibration done every six months following. The liquid water content of the IRT has maintained stability within the stated specifications of variation within +/- 10% of the curve fit equation generated from calibration data. Using past measurements and data trends, IRT characterization engineers wanted to develop methods for the ability to know when data were not within variation. Trends can be observed in the liquid water content measurement process by constructing statistical process control charts. This paper describes data processing procedures for the Multi-Element Sensor in the IRT, including collision efficiency corrections, canonical correlation analysis, process for rejection of data, and construction of control charts.

A process of using machine learning to segment impact ice microstructure is presented and analyzed. The microstructure of impact ice has been shown to correlate with the adhesion strength of ice. Machine vision techniques are explored as a method of decreasing analysis time. The segmentation was conducted with the goal of obtaining average grain size estimations. The model was trained on a set of micrographs of impact ice grown at NASA Glenn’s Icing Research Tunnel. The model leveraged a model pre-trained on a large set of micrographs of various materials as a starting point. Post-processing of the segmented images was done to connect broken boundaries. An automatic method of determining grain size following an ASTM standard was implemented. Segmentation results using different training sets as well as different encoder and decoder pairs are presented. Calculated sizes are compared to manual grain size measurement methods.

Operational issues encountered by Apollo astronauts relating to lunar dust were catalogued, including material abrasion that resulted in scratches and wear on spacesuit components, ultimately impacting visibility, joint mobility and pressure retention. Standard methods are being developed to measure abrasive wear on candidate construction materials to be used for spacesuits, spacecraft, and robotics. Calibration tests were conducted using a standard diamond stylus scratch tip on the common spacecraft structure aluminum, Al 6061-T6. Custom tips were fabricated from terrestrial counterparts of lunar minerals for scratching Al 6061-T6 and comparing to standard diamond scratches. Considerations are offered for how to apply standards when selecting materials and developing dust mitigation strategies for lunar architecture elements.

Oxygen storage and delivery systems for advanced Lunar Exploration Missions are substantially different than those of the International Space Station (ISS) or Apollo missions. The oxygen must be stored without venting for durations of 180 to 210 days prior to use and then used to supply both the steady, low pressure oxygen for the crew, and the higher-pressure oxygen for the extra-vehicular mobility unit. The baseline design is a high pressure gaseous oxygen storage system. Alternate technologies that may offer substantial advantages in terms of the equivalent system mass over the baseline design are being currently evaluated. This study examines both the supercritical and subcritical liquid oxygen storage options, including one with active cooling using a cryocooler. It is found that an actively cooled sub-critical storage system offered the lowest mass system that could satisfy the requirements.

A protocol has been developed that produced the type of lunar soil abrasion damage observed on Apollo spacesuits. This protocol was then applied to four materials (Kevlar®, Vectran®, Orthofabric, and Tyvek®) that are candidates for advanced spacesuits. Three of the four new candidate fabrics (all but Vectran®) were effective at keeping the dust from penetrating to layers beneath. In the cases of Kevlar® and Orthofabric this was accomplished by the addition of a silicone layer. In the case of Tyvek®, the paper structure was dense enough to block dust transport. The least abrasive damage was suffered by the Tyvek®. This was thought to be due in large part to its non-woven paper structure. The woven structures were all abraded where the top of the weave was struck by the abrasive. Of these, the Orthofabric suffered the least wear, with both Vectran® and Kevlar® suffering considerably more extensive filament breakage.

This paper presents results from a smoke detection experiment entitled Smoke Aerosol Measurement Experiment (SAME) which was conducted in the Microgravity Science Glovebox on the International Space Station (ISS) during Expedition 15. Five different materials representative of those found in spacecraft were pyrolyzed at temperatures below the ignition point with conditions controlled to provide repeatable sample surface temperatures and air flow conditions. The sample materials were Teflon®, Kapton®, cellulose, silicone rubber and dibutylphthalate. The transport time from the smoke source to the detector was simulated by holding the smoke in an aging chamber for times ranging from 10 to1800 seconds. Smoke particle samples were collected on Transmission Electron Microscope (TEM) grids for post-flight analysis.

The thick oxide layer of silicon-on-insulator (SOI) devices significantly reduces the junction leakage current at elevated temperatures compared to similar Si devices, resulting in an elevated maximum operating temperature. The maximum operating temperature, specified by manufacturers, of commercial SOI devices/circuits with conventional packaging is usually 225°C. It is important to understand the performance and de-ratings of these SOI circuits at temperatures above 225°C without the temperature limit imposed by commercial packaging technology. This work tested a low frequency square-wave oscillator based on an SOI 555 Timer with a special high temperature ceramic packaging technology from room temperature to 375°C. The timer die was attached to a 96% aluminum oxide substrate with high temperature durable gold (Au) thick-film metallization, and interconnected with Au wires.

The NASA Glenn Research Center has been developing a spacecraft open loop spray evaporative heat sink for use in pressure environments near sea-level, where evaporative cooling of water is not effective. The working fluid is R134a, a common refrigerant used in household appliances, considered safe and non-toxic for humans. The concept uses an open loop spray of R134a impinging on a heated flat plate, through which a closed loop of hot coolant flows, having acquired the heat from spacecraft electronics boxes, the cabin heat exchanger, and other heat sources. The latent heat of evaporation cools the outside of the hot plate, and through heat conduction, reduces the temperature of the coolant. The testing at NASA Glenn has used an electrically heated cylindrical copper target to simulate the hot plate. This paper will discuss the R134a feed system, the test matrix, and test results.

An experiment was conducted in the Icing Research Tunnel (IRT) at NASA Glenn Research Center to study the effect of sweep angle and temperature on the formation of ice accretions on a NACA 0012 swept wing at SLD conditions. From a baseline Appendix-C condition with a MVD of 20m the drop size was changed to 110 and 200m for the SLD cases. Casting data, ice shape tracings, time-sequence and photographic data were obtained. Time-sequence photography was taken during each run to capture in real time the formation of the ice accretion. Measurements of the critical distance were obtained.

A Distributed Engine Control Working Group (DECWG) consisting of the Department of Defense (DoD), the National Aeronautics and Space Administration (NASA)- Glenn Research Center (GRC) and industry has been formed to examine the current and future requirements of propulsion engine systems. The scope of this study will include an assessment of the paradigm shift from centralized engine control architecture to an architecture based on distributed control utilizing open system standards. Included will be a description of the work begun in the 1990's, which continues today, followed by the identification of the remaining technical challenges which present barriers to on-engine distributed control.

The Vapor Phase Catalytic Ammonia Removal (VPCAR) system is being developed to recycle water for future NASA Exploration Missions [1,2,3,4,5]. Reduced gravity testing of the VPCAR System has been initiated to identify any potential problems with microgravity operation. Two microgravity testing campaigns have been conducted on NASA's C-9B Reduced Gravity Aircraft. These tests focused on the fluid dynamics of the unit's Wiped-Film Rotating Disk (WFRD) evaporator. The experiments used a simplified system to study the process of forming a thin film on a rotating disk. The configuration simulates the application of feed in the VPCAR's WFRD evaporator. The first round of aircraft testing, which was completed in early 2006, indicated that a problem with microgravity operation of the WFRD existed. It was shown that in reduced gravity the VPCAR wiper did not produce a uniform thin film [6]. The film was thicker near the axis of rotation where centrifugal forces are small.

Spacecraft radiators reject heat to their surroundings. Radiators can be deployable or mounted on the body of the spacecraft. NASA's Crew Exploration Vehicle is to use body mounted radiators. Coatings play an important role in heat rejection. The coatings provide the radiator surface with the desired optical properties of low solar absorptance and high infrared emittance. These specialized surfaces are applied to the radiator panel in a number of ways, including conventional spraying, plasma spraying, or as an appliqué. Not specifically designed for a weathering environment, little is known about the durability of conventional paints, coatings, and appliqués upon exposure to weathering and subsequent exposure to solar wind and ultraviolet radiation exposure. In addition to maintaining their desired optical properties, the coatings must also continue to adhere to the underlying radiator panel.

This paper will discuss the status of the Compact Flash Evaporator System (CFES) development at NASA Glenn. Three alternative heat sink technologies are being developed under Thermal Control for Advanced Capabilities within the Exploration Technology Development Program. One of them is CFES, a spray cooling concept related to the current Space Shuttle Orbiter Flash Evaporator System (FES). In the CFES concept, water is sprayed on the outside of a flat plate heat exchanger, through which flows the vehicle's primary vehicle heat transfer fluid. The steam is then exhausted to space in an open-loop system. Design, fabrication and testing of the CFES at NASA's Glenn Research Center will be reported.

The on-demand production of Medical Grade Water (MGW) is a critical biomedical requirement for future long-duration exploration missions. Potentially, large volumes of MGW may be needed to treat burn victims, with lesser amounts required to reconstitute pharmacological agents for medical preparations and biological experiments, and to formulate parenteral fluids during medical treatment. Storage of MGW is an untenable means to meet this requirement, as are nominal MGW production methods, which use a complex set of processes to remove chemical contaminants, inactivate all microorganisms, and eliminate endotoxins, a toxin originating from gram-negative bacteria cell walls. An innovative microgravity compatible alternative, using a microwave-based MGW generator, is described in this paper. The MGW generator efficiently couples microwaves to a single-phase flowing stream, resulting in super-autoclave temperatures.

Tests designed to quantify the gravitational effects on thermal mixing and reactant injection in a Supercritical Water Oxidation (SCWO) reactor have recently been performed in the Zero Gravity Facility (ZGF) at NASA's Glenn Research Center. An artificial waste stream, comprising aqueous mixtures of methanol, was pressurized to approximately 250 atm and then heated to 450°C. After uniform temperatures in the reactor were verified, a controlled injection of air was initiated through a specially designed injector to simulate diffusion limited reactions typical in most continuous flow reactors. Results from a thermal mapping of the reaction zone in both 1-g and 0-g environments are compared. Additionally, results of a numerical model of the test configuration are presented to illustrate first order effects on reactant mixing and thermal transport in the absence of gravity.

The Vapor Phase Catalytic Ammonia Removal (VPCAR) system is being developed to recycle water for future NASA Exploration Missions. Testing was recently conducted on NASA's C-9B Reduced Gravity Aircraft to determine the microgravity performance of a key component of the VPCAR water recovery system. Six flights were conducted to evaluate the fluid dynamics of the Wiped-Film Rotating Disk (WFRD) distillation component of the VPCAR system in microgravity, focusing on the water delivery method. The experiments utilized a simplified system to study the process of forming a thin film on a disk similar to that in the evaporator section of VPCAR. Fluid issues are present with the current configuration, and the initial alternative configurations were only partial successful in microgravity operation. The underlying causes of these issues are understood, and new alternatives are being designed to rectify the problems.

Special coatings are being developed and tested to contend with the effects of dust on the lunar surface. These coatings will have wide applicability ranging from prevention of dust buildup on solar arrays and radiator surfaces to protection of EVA space suit fabrics and visors. They will be required to be durable and functional based on application. We have started preparing abrasion-resistant transparent conductive coatings ∼40 nm thick were formed by co-deposition of titanium dioxide (TiO2) and titanium (Ti) on room-temperature glass and polycarbonate substrates using two RF magnetron sputtering sources. By adjusting Ti content, we obtained sheet resistivities in the range 104-1010 ohms/square. We have also started conducting a series of environmental tests that simulate the exposure of coated samples to dust under relevant conditions, beginning with abrasion tests using regolith simulant materials.

Supercritical water oxidation (SCWO) may become an attractive technology for processing solid and liquid wastes for long duration space and extraterrestrial planetary missions. Gravitational influences on the operation of SCWO reactors are discussed in the context of key dimensionless parameters for two general modes of operation: a “premixed” mode, where the reactants are brought to supercritical temperatures and pressures simultaneously, and a “diffusion limited” mode, where one of the reactants (typically the oxidizer) is injected into the reactor after the bulk fluid is raised to supercritical temperatures and pressures. An experimental facility for testing the gravitational influences on a SCWO reactor is then discussed.

Packed bed reactors are well known for their vast and diverse applications in the chemical industry; from gas absorption, to stripping, to catalytic conversion. Use of this type of reactor in terrestrial applications has been rather extensive because of their simplicity and relative ease of operation. Developing similar reactors for use in microgravity is critical to many space-based advanced life support systems. However, the hydrodynamics of two-phase flow packed bed reactors in this new environment and the effects of one physicochemical process on another has not been adequately assessed. Surface tension or capillary forces play a much greater role which results in a shifting in flow regime transitions and pressure drop. Results from low gravity experiments related to flow regimes and two-phase pressure drop models are presented in this paper along with a description of plans for a flight experiment on the International Space Station (ISS).

Using a new fiber electrode technology, currently developed and produced by Bekaert Corporation (Bekaert), Electro Energy, Inc., (EEI) Mobile Energy Products Group (formerly, Eagle-Picher Technologies, LLC, Power Systems Department) in Colorado Springs, CO has demonstrated that it is feasible to manufacture flight weight nickel hydrogen cells having about twice the specific energy (80 vs. 40 watt-hr./kg) as state-of-the-art nickel hydrogen cells that are currently flown on geosynchronous communications satellites. Although lithium-ion battery technology has made large in-roads to replace the nickel alkaline technology (nickel-cadmium, nickel-metal hydride), the technology offered here competes with lithium-ion weight and offers alternatives not present in the lithium-ion chemistry such as: ability to undergo a continuous overcharge, reversal on discharge, and sustain rate capability sufficient to start automotive and aircraft engines at subzero temperatures.