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The selection of parameters during friction stir spot welding of Al-alloys and Mg-alloys is discussed. The role of tool rotation speed, plunge rate, and dwell time is examined in relation to the tool heating rate,temperature, force, and torque that occur during spot welding. In order to reduce the cycle time and tool force during Al- alloy spot welding, it is necessary to increase the tool rotation speed >1500 RPM. The measured peak temperature in the stir zone is determined by the rotation speed and dwell time, and is ultimately limited by the solidus of the alloy. When tool rotation speeds >1500 RPM are employed during AZ91 Mg-alloy spot welding, the tendency for melted film formation and cracking are greatly increased.

Friction stir spot welding of Mg-alloy AZ91 is investigated. The temperature cycles within the stir zone and in the TMAZ region are examined using thermocouples, which are located within the tool itself and also by locating thermocouples in drilled holes at specific locations relative to the bottom of the tool shoulder and the periphery of the rotating pin. The measured temperatures in the stir zone range from 437°C to 460°C (0.98Ts, where Ts is the solidus temperature in degrees Kelvin) in AZ91 spot welds produced using plunge rates from 2.5 and 25 mm/s. The thermal cycle within the stir zone formed during AZ91 spot welding could not be measured by locating thermocouples within the workpiece in drilled holes adjacent to the periphery of the rotating pin.

Energy generation and utilization during friction stir spot welding of Al 6061-T6 and AM50 sheet materials are investigated. The dimensions of the stir zones during plunge testing are largely unchanged when the tool rotational speed increases from 1500 RPM to 3000 RPM (for a plunge rate of 1 mm/s) and when the rate of tool penetration increases from 1 mm/s to 10 mm/s (for a tool rotational speed of 3000 RPM). The energy resulting from tool rotation is also unaffected when higher tool rotational speeds are applied. The rotating pin accounts for around 70% and 66% of the energy generated when 6.3 mm thick Al 6061-T6 and AM50 sheet materials are spot welded without the application of a dwell period. In direct contrast, the contribution made by the tool shoulder increases to around 48% (Al 6061-T6) and to 65% (AM50) when a four second long dwell period is incorporated during spot welding of 6.3 mm thick sheets.

This work is based on a process to develop novel cellulose microfibre reinforced composite materials, and to understand fundamental mechanical properties of these composites. Cellulose microfibres having diameters <1 μm were generated from bleached kraft pulp by a combination of high shear refining and subsequent cryocrushing under liquid nitrogen, followed by filtration through a 60 mesh screen. Through film casting in polyvinyl alcohol, theoretical stiffness of the microfibres was calculated as 69 GPa. Subsequently, these microfibres were successfully dispersed in the bioplastics thermoplastic starch and polylactic acid (PLA), using conventional processing equipments. The high aspect ratio of these microfibres coupled with their high tensile properties imparted superior mechanical strength and stiffness to the composites. These indicated that by suitably choosing the polymer, excellent reinforcement can be achieved for high end applications like automotive parts.

The use of natural fibers for polymer composite materials has increased tremendously in the last few years. This type of reinforcements offers many advantages such as low density, low cost, high specific strength and low environmental impacts. The performance of the natural fiber composites are affected by the fiber loading, the individual mechanical properties of each component (fiber and matrix), and the fiber and matrix adhesion. Concerning the interfacial interaction, natural fibers present a major drawback because of poor compatibility of fibers with most hydrophobic thermoplastic and thermoset matrix. Hemp fiber/acrylic composites were manufactured with sheet molding technique recently. Although mechanical tests give promising results, they exhibit low tensile strength resulting from a poor fiber/matrix adhesion. The moisture resistance property of the sheet molded composites also needs further improvement.

This paper demonstrates the effects of nano-clay on the microcellular foam processing of nylon. First, Nylon 6 nanocomposites with 1 wt% clay were prepared by a twin screw extruder. The nanocomposite structures were characterized by XRD and TEM. Nylon and its nanocomposites were foamed in extrusion using CO2. The cell morphologies of nylon and its nanocomposite foams were investigated. It appeared that the nano-clay not only enhanced cell nucleation, but also suppressed cell deterioration in the microcellular foaming of nylon.

Eco-efficient and cost effective natural fibre - thermoplastic composites have gained attention to a great extent in the automotive industry. Most of the OEM specifications for automotive interior parts, for example, instrument panels, recommend the composite should have a minimum flexural modulus of 1900 MPa, a notched Impact strength greater than 150 J/m at room temperature and a melt flow index of 5 g/10min and above [1, 2 and 3]. The objective of this work was to develop a high performance hybrid composite by injection molding process of the composites made from natural fibre in combination with glass fibre or calcium carbonate in a thermoplastic matrix to meet the specifications required for automotive interior parts applications. Mechanical properties, such as tensile and flexural strengths and moduli of the composites prepared, were found to be highly promising.

In this work hemp fibers were chemically treated in order to improve the fiber/matrix interaction in hemp fiber/unsaturated polyester composites prepared by a Resin Transfer Molding (RTM) process. Chemicals used for paper sizing (AKD, ASA, Rosin Acid and SMA) as well as a silane compound and sodium hydroxide were used to modify the fibers' surface. The tensile, flexural and impact properties of the resulting materials were measured. A slight improvement in mechanical properties was observed for the SMA, silane and alkali treated specimens. However close analysis of these tests and of the fracture surface of the samples showed that there was no amelioration of the fiber/matrix adhesion. It was found that predicted tensile strengths using the rule of mixture were very close to the experimental values obtained in this work. Finally the properties of an hybrid glass fiber/hemp fiber composite were found to be very promising