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An experimental study of the Homogeneous Charge Compression Ignition (HCCI) combustion process has been conducted by using chemiluminescence imaging. The major intent was to characterize the flame structure and its transient behavior. To achieve this, time resolved images of the naturally emitted light were taken. Emitted light was studied by recording its spectral content and applying different filters to isolate species like OH and CH. Imaging was enabled by a truck-sized engine modified for optical access. An intensified digital camera was used for the imaging. Some imaging was done using a streak-camera, capable of taking eight arbitrarily spaced pictures during a single cycle, thus visualizing the progress of the combustion process. All imaging was done with similar operating conditions and a mixture of n-heptane and iso-octane was used as fuel. Some 20 crank angles before Top Dead Center (TDC), cool flames were found to exist.