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In this study, effects of altitude on free diesel spray morphology, macroscopic spray characteristics and air-fuel mixing process were investigated. The diesel spray visualization experiment using high-speed photography was performed in a constant volume chamber which reproduced the injection diesel-like thermodynamic conditions of a heavy-duty turbocharged diesel engine operating at sea level and 1000 m, 2000 m, 3000 m and 4500 m above sea level. The results showed that the spray morphology became narrower and longer at higher altitude, and small vortex-like structures were observed on the downstream spray periphery. Spray penetration increased and spray angle decreased with increasing altitude. At altitudes of 0 m, 1000 m, 2000 m, 3000 m and 4500 m, the spray penetration at 1.45 ms after start of injection (ASOI) were 79.54 mm, 80.51 mm, 81.49 mm, 83.29 mm and 88.92 mm respectively, and the spray angle were 10.9°, 10.8°, 10.7°, 10.4°and 9.8° respectively.