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Technical Paper

Ash Storage Capacity Enhancement of Diesel Particulate Filter

2004-03-08
2004-01-0949
The life of DPF would be decided by ash durability because pressure loss of DPF is increased by accumulation of ash that is produced when soot is burnt in the DPF. We could succeed to increase maximum ash capacity and extend the life of the DPF by an approach from the filter design, making inlet cell volume larger than outlet cell. Furthermore, when the inlet cell is designed octagon, we found that slanted wall blocking the inlet cells is functional worked for soot filtration. As the results, we could improve to manage both transient pressure loss while the soot is collected and the ash durability by the cell shape with (inlet cell/outlet cell) = (octagon/square).
Technical Paper

Characterization of High Porosity SiC-DPF

2002-03-04
2002-01-0325
The pore diameter and porosity of SiC-DPF has been increased by elaborating its porous structure. Increasing the porosity of DPF decreases its strength and thermal conductivity. It was clarified how these characteristics affect the performance such as filtration characteristics, low pressure loss, maximum soot loading limit, and thermal response characteristics required for DPF. It was found that the basic characteristics of SiC such as high strength and high thermal conductivity play an important role in its high porosity.
Technical Paper

Characterization of Thin Wall SiC-DPF

2003-03-03
2003-01-0377
We examined a filter structure of a SiC-DPF, and found that the reduction in a wall thickness is effective in decreasing a pressure loss. And we made it clear how this reduction in the wall thickness influences the performances of the DPF, that are the filtration efficiency and the accumulated soot mass limit which are important for the DPF. From the results of this study, it can be seen that the filter structure which is suitable for the catalyzed DPF should be controlled in a porosity and the wall thickness in proportion to an amount of catalyst required.
Technical Paper

Development of High Porosity SiC-DPF Which is Compatible with High Robustness and Catalyst Coating Capability for SCR Coated DPF Application

2013-04-08
2013-01-0840
Diesel emission regulation becomes stringent more and more regarding both particulate matter (PM) and NOx in the worldwide. SCR coated DPF system is considered as one of the promising options for future diesel exhaust after-treatment because it has several benefits such as the downsizing of the system, quick light-off of the catalytic function due to mounting closed-couple position. To integrate the SCR converter into the DPF, it is necessary to design the DPF substrate's porosity higher and pore size larger than conventional DPF to improve SCR catalyst coating capability. However to make the porosity higher will lose the robustness in general. Against these problems, it was studied to improve the high porosity DPF performances by applying the new technology to modify the thermal shock resistance property.
Technical Paper

Durability of Filtration Layers Integrated into Diesel Particulate Filters

2013-04-08
2013-01-0837
This paper describes the durability of the filtration layer integrated into Diesel Particulate Filters (DPFs) that we have developed to ensure low pressure loss and high filtration efficiency performances which also meet emission regulations. DPF samples were evaluated in regards to their performance deterioration which is brought about by ash loading and uncontrolled regeneration cycles, respectively. Ash was synthesized by using a diesel fuel/lubrication oil mixture and was trapped up to a level which corresponded to a 240,000km run, into the DPFs both with and without the filtration layer. Afterwards, aged-DPFs were measured with respect to their permeability, pressure loss, filtration efficiency, as well as soot oxidation speed using suitable analytical methods. Consequently, it has been confirmed that there was no noteworthy deterioration of the performances in the DPF with the filtration layer.
Technical Paper

Experimental Study of Physical and Chemical Properties of Soot under Several EGR Conditions

2014-04-01
2014-01-1593
Exhaust Gas Recirculation (EGR) is an effective method to reduce Nitrogen Oxide emissions. In recent years the trend of increasing EGR rate in-cylinders is an integral part of most improvements in combustion technology developments. The object of this work is to study the influence of EGR rate on the physical and chemical properties of soot particles. Soot from several operating points of a diesel engine run were collected on a high temperature filters. The pressure drop behavior during the soot loading was monitored then the soot permeability was calculated. Afterwards, the soot primary size was calculated from the obtained data and it showed good correspondence to the actual measurement. It is confirmed that all the soot primary sizes were around 22 nm in diameter. In contrast, the soot aggregate sizes and the soot concentrations were found to increase with increasing EGR rate. Subsequently, Oxidation tests were conducted to evaluate the reactivity of the soot.
Technical Paper

Further Durability Enhancement of Re-crystallized SiC-DPF

2004-03-08
2004-01-0954
SiC has very high thermal conductivity and mechanical strength. The cracking problem during regeneration could be successfully handled by using split-type DPFs that consist of multiple filter segments. For enhancing further durability of SiC-DPF, increasing the regeneration limit was successful by means of increasing a volume of the neck area located between SiC particles. The improvement was probably due to the lowering of Young's modulus and increasing of the thermal shock fracture resistance parameter R', which were results of increasing the neck volume and controlling the sintering method. Crack propagation mode changed from the conventional mode, and the cracks propagating throughout the whole tended to be restrained.
Technical Paper

Further Experimental Study of Asymmetric Plugging Layout on DPFs: Effect of Wall Thickness on Pressure Drop and Soot Oxidation

2015-04-14
2015-01-1016
In order to guide the development of asymmetric plugging layout Diesel Particulate Filters, hereafter referred to as “VPL-DPF”, in this paper we present some evaluation results regarding the effect of design parameters on the VPL-DPF performance. VPL-DPF samples which have different wall thicknesses (thin and thick walls) were evaluated in regards to their pressure drop and soot oxidation behaviors, with the aim to optimize the design of DPF structure. As a result of pressure drop evolution during soot loading, contrary to our expectation, in some cases, it was found out that VPL increases the transient pressure drop compared to the conventional plugging layout DPF. That meant there is an appropriate specific optimum wall thickness for adoption of VPL which has to be well defined at its structural design phase. Based on our previous research, it is expected that this result is due to interactions among the different (five) wall flows that exist in a VPL-DPF.
Technical Paper

Improving of the Filtration and Regeneration Performance by the Sic-DPF with the Layer Coating of PM Oxidation Catalyst

2008-04-14
2008-01-0621
DPF has become widely known as an indispensable after-treatment component for the purification of the particulate matter in the diesel exhaust gas. But, in order to correspond to further regulation strengthening such as carbon dioxide emission regulation and number-based particulate matter emission regulation, it must be necessary also for DPF to keep improving its performance. In this study, it was examined how to improve both the filtration efficiency and the oxidation efficiency of PM regarding the catalyzed DPF. SiC-made 10mil/300cpsi-OctoSquare asymmetric cell structure was chosen for the DPF substrate and PM oxidation catalyst was coated on the surface of the filter wall as a layer with the device of the coating method. As a result, it was found that the layer coated DPF has advantage on the filtration efficiency without soot accumulation and efficiency was similar to an uncoated one with 0.1 g/l soot loading.
Technical Paper

Performance Evaluation of SiC-DPF Sintered with Sintering Additive

2005-04-11
2005-01-0579
SiC is well known as a ceramic with high mechanical strength and thermal conductivity, and the R-SiC-DPF (recrystallized SiC-DPF) used these excellent properties is widely recognized as the substrate material for DPF. DPF system requires the material possessing high thermal shock resistance against an unexpected accident, such as an uncontrolled regeneration. One of the indices indicating the thermal shock resistance of the DPF is soot mass limit, which is an important factor determining the penalty of vehicle fuel consumption. In order to further increase the soot mass limits of R-SiC-DPF, this paper covers the attempts of IBIDEN to promote the sintering of the neck part of a SiC porous body using a sintering additive. Al2O3, well known as a sintering additive for a SiC dense body, was selected as the sintering additive.
Technical Paper

Soot Loading Estimation Accuracy Improvement by Filtration Layer Forming on DPF and New Algorithm of Pressure Loss Measurement

2013-04-08
2013-01-0525
A diesel particulate filter (DPF) is a key component for reduction of engine soot emission. The soot collected in the DPF is periodically burned off, so-called DPF regeneration, and a behavior of the pressure drop increased by the soot loading is generally utilized to estimate the amount, which must be a trigger of the regeneration. However, it is said that the estimation of the soot loading amount has considerable dispersion caused by two main reasons. One is hysteresis of the transient pressure drop resulted from the combination of so-called deep-bed and cake filtration modes. The other is a fluctuation of exhaust gas temperature and flow rate as well as a pulsation from the engine. In this study, the accurate estimation method of the soot amount accumulated in the DPF was proposed in combination with filtration layers (FLs) technology and a new algorithm based on fast Fourier transform (FFT) technology.
Technical Paper

Soot Oxidation Kinetics in Diesel Particulate Filters

2007-04-16
2007-01-1129
Direct catalytic soot oxidation is expected to become an important component of future diesel particulate emission control systems. The development of advanced Catalytic Diesel Particulate Filters (CDPFs relies on the interplay of chemistry and geometry in order to enhance soot-catalyst proximity. An extensive set of well-controlled experiments has been performed to provide direct catalytic soot oxidation rates in CDPFs employing small-scale side-stream sample exposure. The experiments are analyzed with a state-of-the-art diesel particulate filter simulator and a set of kinetic parameters are derived for direct catalytic soot oxidation by fuel-borne catalysts as well as by catalytic coatings. The influence of soot-catalyst proximity, on catalytic soot oxidation is found to be excellently described by the so-called Two-Layer model, developed previously by the authors.
Technical Paper

Study on Catalyzed-DPF for Improving the Continuous Regeneration Performance and Fuel Economy

2007-04-16
2007-01-0919
It is a big challenge how to satisfy both the purification of exhaust gas and the decrease of fuel penalty, that is, carbon-dioxide emission. Regarding the Diesel Particulate Filter (DPF) applied in the diesel after-treatment system, it must be effective for lowering the fuel penalty to prolong the interval and reduce the frequency of the DPF regeneration operation. This can be achieved by a DPF that has high Particulate Matter (PM) mass limit and high PM oxidation performance that is enough to regenerate the DPF continuously during the normal running operation. In this study, the examination of the pore structure of the wall of a DPF that could expand the continuous regeneration region in the engine operation map was carried out. Several porous materials with a wide range of pore structure were prepared and coated with a Mixed Oxide Catalyst (MOC). The continuous regeneration performance was evaluated under realistic conditions in the exhaust of a diesel engine.
Technical Paper

Study on Filter Substrate Structure for Lower Backpressure and Higher Regeneration Performance

2006-04-03
2006-01-1526
The trade-off between NOx and particulate matter (PM) has been a technological challenge with respect to diesel engine emissions. However, the practical use of diesel particulate filters (DPF) has made diesel emission control possible, in which NOx emissions are reduced through engine control and nearly all emitted PM is completely removed by DPF from diesel exhaust emissions. This has helped to contribute to laying the foundation for pursuing of the high theoretical thermal efficiency of diesel engines. However, it is also a fact that such emission controls have resulted in considerable impairments on the original and greatest advantages of diesel engines. This includes fuel penalties with accompanying increases in fuel consumption caused by pressure losses due to the attachment of the DPF itself and the accumulation of PM in the DPF, as well as fuel losses that occur when fuel is used to regenerate collected PM.
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