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This paper reports on the third part of a continued study (SAE Papers 961182, 971636) to develop the Ignition Quality Tester (IQT™). Past research has shown that this automated laboratory/refinery apparatus can be used to accurately predict the cetane number of middle distillates and alternative fuels using small sample volumes (< 50 mL). The paper reports on the main objective of a study performed by Advanced Engine Technology Ltd. (AET), in co-operation with its research partners. The primary research objective of this work is to further the understanding of fuel preparation (fuel air mixing) and start of combustion processes in the IQT™. Key to this understanding is the manner in which single molecule compounds and full boiling-range diesel fuels behave during these processes. Insights are provided into the manner in which the American Society for Testing and Materials (ASTM) D-613 primary reference fuels (PRFs) undergo fuel preparation and start of combustion in the IQT™.

Four major coal fuel projects which were performed at Southwest Research Institute over the past ten years are reviewed. Beginning with the “Alternative Fuels for Highway Utilization” project in 1979, and the success of carbon-black/diesel fuel slurries, the development of the coal slurries is traced to the current technology. Most recently, full-scale locomotive engines have been operated on 50% coal in water slurries at thermal efficiencies approaching that of diesel fuel performance. The paper is concluded with a recommended engine design for coal slurries.

A technique is verified for mapping the exhaust emission levels of a diesel engine during transient operation. Particulate matter, oxides of nitrogen, hydrocarbons, and carbon monoxide emissions were sampled for discrete segments of various transient cycles. Each cycle consisted of four distinct segments. The discrete segments are described by average engine conditions, rate of change variables, and segment length. Regression analysis was used to develop equations relating the emission levels during each segment to the engine parameters. The regression equations were then used to obtain estimates of composite emission levels of several complex transient cycles that were subsequently tested. These cycles included the EPA heavy-duty transient cycle and two simulated heavy-duty cycles developed for underground mine vehicles. Comparison of the predicted and measured cycle emissions are made for the EPA heavy duty cycle and the simulated mine cycles.

Slurry fuels of various forms of solids in diesel fuel were developed and evaluated for their relative potential as fuel for diesel engines. Thirteen test fuels with different solids concentrations were formulated using eight different materials. The injection and atomization characteristics (transient diesel sprays) of the test fuels were examined in a spray bomb in which a nitrogen atmosphere was maintained at high pressure and temperature, 4.2 MPa and 480°C, respectively. The diagnostics of the sprays included high-speed movies and high-resolution still photographs. The slurries were also tested in a single-cylinder CLR engine in both direct-injection and prechamber configurations. The data included the normal performance parameters as well as heat release rates and emissions. In most cases, the slurries performed very much like the baseline fuel. The combustion data indicated that a large fraction (90 percent or more) of the solids were burning in the engine.

The ignition delay times of forty-two different fuels were measured in a constant volume combustion bomb. The measurements were performed at three different initial air temperatures using fuels ranging from the primary reference fuels for cetane rating to complex mixtures of coal-derived liquids. The ignition delay times were examined in terms of the classical definitions of the physical and chemical delay times. The previously used definitions were found to be inadequate, and new definitions have been proposed. The total ignition delay times were studied in the context of providing a means for rating the ignition quality of the fuels. Fuel ignition quality rating schemes are discussed, including one based on the current cetane number scale as well as one based on a new scale which includes a measure of the sensitivity of the various fuels to the air temperature.

A combustion-based analytical method, initially developed by the Southwest Research Institute (SwRI) referred to as the Constant Volume Combustion Apparatus (CVCA), has been further researched/developed by an SwRI licensee (Advanced Engine Technology Ltd.) as an Ignition Quality Tester (IQT) for laboratories and refineries. The IQT software/hardware system permits rapid and precise determination of ignition quality for middle distillate fuels. Its features, such as low fuel volume requirement, complete test automation, and self-diagnosis, make it highly suitable for commercial oil industry and research applications. Operating and test conditions were examined in the context of providing a high correlation with cetane number (CN), as determined by the ASTM D-613 method. Preliminary investigation indicates that the IQT results are highly repeatable (± 0.30 CN), providing a high sensitivity to CN variation over the 33 to 58 CN range.

A combustion-based analytical method, initially developed by the Southwest Research Institute (SwRI) and referred to as the Constant Volume Combustion Apparatus (CVCA), has been further researched/developed by an SwRI licensee (Advanced Engine Technology Ltd.). This R&D has resulted in a diesel fuel Ignition Quality Tester (IQT) that permits rapid and precise determination of the ignition quality of middle distillate and alternative fuels. Its features, such as low fuel volume requirement, complete test automation, and self-diagnosis, make it highly suitable for commercial oil industry and research applications. A preliminary investigation, reported in SAE paper 961182, has shown that the IQT results are highly correlated to the ASTM D-613 cetane number (CN). The objective of this paper is to report on efforts to further refine the original CN model and report on improvements to the IQT fuel injection system.

This paper reports on the fourth part of a continued study on further research and development with the automated Ignition Quality Tester (IQT™). Research over the past six years (reported in SAE papers #961182, 971636 and 1999-01-3591) has demonstrated the capabilities of this automated apparatus to measure the ignition quality and accurately determine a derived cetane number (DCN) for a wide range of middle distillate and non-conventional diesel fuels. The present paper reports on a number of separate investigations supporting these continued studies.

Twelve different hole shapes for diesel injector tips were characterized with DF-2 diesel fuel for spray cone angle over a range of injection pressures from 21 MPa (3 kpsi) to 69 MPa (10 kpsi). A baseline and two of the most radical designs were also tested for drop-size distribution and liquid volume fraction (liquid fuel-air ratio) over a range of pressures from 41 MPa (6 kpsi) to 103 MPa (15 kpsi). All hole shapes were circular in cross-section with minimum diameters of 0.4 mm (0.016 in.), and included converging and diverging hole shapes. Overall hole lengths were constant at 2.5 mm (0.098 in.), for an L/d of 6.2. However, the effective L/d may have been less for some of the convergent and divergent shapes.

The specific goal of this project was to determine if there is a difference in the lube oil degradation rates in a heavy-duty diesel engine equipped with an EGR system, as compared to the same configuration of the engine, but minus the EGR system. A secondary goal was to develop FTIR analysis of used lube oil as a sensitive technique for rapid evaluation of the degradation properties of lubricants. The test engine selected for this work was a Caterpillar 3176 engine. Two engine configurations were used, a standard 1994 design and a 1994 configuration with EGR designed to meet the 2004 emissions standards. The most significant changes in the lubricant occurred during the first 50-100 hours of operation. The results clearly demonstrated that the use of EGR has a significant impact on the degradation of the engine lubricant.

Several diesel injection systems were selected for evaluating the effects of fuel properties on diesel spray characteristics. Fuel properties that were examined were viscosity and specific gravity. The selected injection systems were operated on nine test fuels covering a broad range of viscosity and specific gravity. High-speed movies were taken of the fuels being injected into a high-pressure environment. Penetration and cone angle data were reduced from the movies and used as a basis for fuel-to-fuel comparisons. In addition, drop size distribution data were obtained for one injection system operating on four fuels with different viscosities. Fuel viscosity was found to have an effect on spray tip penetration. For a pintle-type nozzle as fuel viscosity increased, the tip penetration rate decreased. Tip penetration rate from a pressure time injection system was proportional to the fuel viscosity, in that as viscosity increased, tip penetration increased.

In-cylinder control of particulate emissions in a diesel engine depends on careful control and understanding of the fuel injection and air/fuel mixing process. It is extremely difficult to measure physical parameters of the injection and mixing process in an operating engine, but it is possible to simulate some diesel combustion chamber conditions in a steady flow configuration whose characteristics can be more easily probed. This program created a steady flow environment in which air-flow and injection sprays were characterized under non-combusting conditions, and emissions measurements were made under combusting conditions. A limited test matrix was completed in which the following observations were made. Grid-generated air turbulence decreased particulates, CO, and unburned hydrocarbons, while CO2 and NOx levels were increased. The turbulence accelerated combustion, resulting in more complete combustion and higher temperatures at the measurement location.

Changing fuel quality, increasingly stringent exhaust emission standards, demands for higher efficiency, and the trend towards higher specific output, all contribute to the need for a better understanding of the ignition process in diesel engines. In addition to the impact on the combustion process and the resulting performance and emissions, the ignition process controls the startability of the engine, which, in turn, governs the required compressions ratio and several of the other engine design parameters. The importance of the ignition process is reflected in the fact that the only combustion property that is specified for diesel fuel is the ignition delay time as indicated by the cetane number. The objective of the work described in this paper was to determine the relationship between the ignition process as it occurs in an actual engine, to ignition in a constant volume combustion bomb.

Homogeneous Charge Compression Ignition (HCCI) experiments were performed in a variable compression ratio single cylinder engine. This is the fourth paper resulting from work performed at Southwest Research Institute in this HCCI engine. The experimental variables, in addition to speed and load, included compression ratio, EGR level, intake manifold pressure and temperature, fuel introduction location, and fuel composition. Mixture preparation and start of reaction control were identified as fundamental problems that required non-traditional mixture preparation and control strategies. The effects of the independent variable on the start of reaction have been documented. For fuels that display significant pre-flame reactions, the start of the pre-flame reactions is controlled primarily by the selection of the fuel and the temperature history of the fuel air mixture.

A single-cylinder, direct-injection diesel engine was modified to operate on compression ignition of homogenous mixtures of diesel fuel and air. Previous work has indicated that extremely low emissions and high efficiencies are possible if ignition of homogeneous fuel-air mixtures is accomplished. The limitations of this approach were reported to be misfire and knock. These same observations were verified in the current work. The variables examined in this study included air-fuel ratio, compression ratio, fresh intake air temperature, exhaust gas recirculation rate, and intake mixture temperatures. The results suggested that controlled homogeneous charge compression ignition (HCCI) is possible. Compression ratio, EGR rate, and air fuel ratio are the practical controlling factors in achieving satisfactory operation. It was found that satisfactory power settings are possible with high EGR rates and stoichiometric fuel-air mixtures.

Diesel engine optimization for low emissions and high efficiency involves the use of very high injection pressures. It was generally thought that increased injection pressures lead to improved fuel air mixing due to increased atomization in the fuel jet. Injection experiments in a high-pressure, high-temperature flow reactor indicated, however, that high injection pressures, in excess of 150 MPa, leads to greatly increased penetration rates and significant wall impingement. An endoscope system was used to obtain movies of combustion in a modern, 4-valve, heavy-duty diesel engine. Movies were obtained at different speeds, loads, injection pressures, and intake air pressures. The movies indicated that high injection pressure, coupled with high intake air density leads to very short ignition delay times, ignition close to the nozzle, and burning of the plumes as they traverse the combustion chamber.

High-speed movie films, and laser-diffraction drop sizing were used to evaluate the structure, penetration rate, cone angle, and drop size distribution of diesel sprays in a constant volume pressure vessel. As further means of evaluating the data, comparisons are made between the film measurements, and calculations from a dense gas jet model. In addition to the high-speed film data that describes the overall structure of the spray as a function of time, a laser diffraction instrument was used to measure drop size distribution through a cross-section of the spray. In terms of the growth of the total spray volume (a rough measure of the amount of air entrained in the spray), spray impingement causes an initial delay, but generally the same overall growth rate as an equivalent unimpeded spray. Agreement between measurements and calculations is excellent for a diesel spray with a 0.15 mm D orifice and relatively high injection pressures.

Because of its dominant role in diesel engine performance and emissions, the fuel injection process has become an area of very active research and development. It is now clear that location, shape, rate of development, and mass flow distribution within each fuel jet are all important in controlling fuel air mixing, wall interactions, combustion rate, and the resulting levels of emissions. The objective of this project was to develop an instrument for measurement of the instantaneous fuel mass and momentum distribution in the jets issuing from diesel injection nozzles. The goal was to develop an instrument concept that can be used in the laboratory for fundamental measurements, as well as a quality control system for use in manufacture of the injection nozzles. The concept of the instrument is based on the measurement of the instantaneous momentum of the fuel jet as it impacts on a surface equipped with pressure sensitive elements.

Methods to reduce direct injected diesel engine emissions in the combustion chamber will be discussed in this paper. The following NOx emission reduction technologies will be reviewed: charge air chilling, water injection, and exhaust gas recirculation (EGR). Emphasis will be placed on the development of an EGR system and the effect of EGR on NOx and particulates. The lower limit of NOx that can be obtained using conventional diesel engine combustion will be discussed. Further reductions in NOx may require changing the combustion process from a diffusion flame to a homogeneous charge combustion system.

This paper explores the possibility of on-board fuel classification for fuel property adaptive compression-ignition engine control system. The fuel classifier is designed to on-board classify the fuel that a diesel engine is running, including alternative and renewable fuels such as bio-diesel. Based on this classification, the key fuel properties are provided to the engine control system for optimal control of in-cylinder combustion and exhaust treatment system management with respect to the fuel. The fuel classifier employs engine input-output response characteristics measured from standard engine sensors to classify the fuel. For proof-of-concept purposes, engine input-output responses were measured for three different fuels at three different engine operating conditions. Two neural-network-based fuel classifiers were developed for different classification scenarios. Of the three engine operating conditions tested, two conditions were selected for the fuel classifier to be active.