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Using synchrotron x-radiography and mass deconvolution techniques, this work reveals strikingly interesting structural and dynamic characteristics of the direct injection (DI) gasoline hollow-cone sprays in the near-nozzle region. Employed to measure the sprays, x-radiography allows quantitative determination of the fuel distribution in this optically impenetrable region with a time resolution of better than 1 μs, revealing the most detailed near-nozzle mass distribution of a DI gasoline fuel spray ever detected. Based on the x-radiographs of the spray collected from four different perspectives, enhanced mathematical and numerical analyses were developed to deconvolute the mass density of the gasoline hollow-cone spray. This leads to efficient and accurate regression curve fitting of the measured experimental data to obtain essential parameters of the density distribution that are then used in reconstructing the cross-sectional density distribution at various times and locations.