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Nanoparticle formation during exhaust sampling and dilution has been examined using a two-stage micro-dilution system to sample the exhaust from a modern, medium-duty diesel engine. Growth rates of nanoparticles at different exhaust dilution ratios and temperatures have been determined by monitoring the evolution of particle size distributions in the first stage of the dilution system. Two methods, graphical and analytical, are described to determine particle growth rate. Extrapolation of size distribution down to 1 nm in diameter has been demonstrated using the graphical method. The average growth rate of nanoparticles is calculated using the analytical method. The growth rate ranges from 6 nm/sec to 24 nm/sec, except at a dilution ratio of 40 and primary dilution temperature of 48 °C where the growth rate drops to 2 nm /sec. This condition seems to represent a threshold for growth. Observed nucleation and growth patterns are consistent with predictions of a simple physical model.

Particle size distribution and number concentration measurements have been made in the diluted exhaust of a medium-duty, turbocharged, aftercooled, direct-injection Diesel engine using a unique variable residence time micro-dilution system that allows systematic variation of dilution and sampling conditions, and a scanning mobility particle sizer (SMPS). The measurements show that the number concentrations in the nanoparticle (Dp < 50 nm) and the ultrafine (Dp < 100 nm) ranges are very sensitive to dilution conditions and fuel sulfur content. Changes in concentration of up to two orders of magnitude have been observed when conditions are varied over the range that might be encountered in typical laboratory dilution systems. For example, at a dilution ratio of 12, dilution temperature of 32 °C, and a residence time of 1000 ms, the number concentrations reach 6 × 108 part.

The third long-term ATES cycle (LT3) was conducted between October 1989 and March 1990. Objectives of LT3 were to demonstrate that high-temperature ATES could supply a real heating load and to simplify the water chemistry modeling. For LT3 the Field Test Facility (FTF) was connected to a nearby campus building to demonstrate the FTF's ability to meet a real heating load. For LT3 the wells were modified so that only the most permeable portions of the Ironton-Galesville aquifer were used to simplify water chemistry comparisons and modeling. The campus steam plant was the source for heat stored during LT3. A total volume of 63.2 x 103 m3 of water was injected at a rate of 54.95 m3/hr into the storage well at a mean temperature of 104.7°C from October through December 1989. Tie-in to the Animal Sciences Veterinary Medicine (ASVM) building was not completed until late December.