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The growing severity of global environmental issues in recent years, including air pollution and the depletion of fossil fuels, has made it necessary for internal combustion engines to achieve higher efficiency and lower exhaust emission levels. Calls for reducing atmospheric emissions of carbon dioxide (CO₂) necessitate thoroughgoing measures to lower the levels of CO₂ originating in the combustion process of internal combustion engines and to facilitate operation on diverse energy sources. Homogeneous Charge Compression Ignition (HCCI) combustion has attracted widespread interest because it achieves high efficiency and can reduce particulate matter (PM) and nitrogen oxide (NOx) emissions simultaneously. These characteristics are obtainable because HCCI combustion can take place at ultra-lean conditions exceeding the limits of flame propagation.

There are strong demands today to further improve the thermal efficiency of internal combustion engines against a backdrop of various environmental issues, including rising carbon dioxide (CO2) emissions and global warming. One factor that impedes efforts to improve the thermal efficiency of spark ignition engines is the occurrence of knocking. The aim of this study was to elucidate the details of knocking based on spectroscopic measurements and visualization of phenomena in the combustion chamber of a test engine that was operated on three primary reference fuels with different octane ratings (0 RON, 30 RON, and 50 RON). The ignition timing was retarded in the experiments to delay the progress of flame propagation, making it easier to capture the behavior of low-temperature oxidation reactions at the time knocking occurred.