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Experimental results focused towards developing tribological surface coatings coupled with liquid lubricant boundary layer effects, for advanced high temperature military diesel engine applications are presented. The primary focus of this work is in the area of advanced, low heat rejection (LHR) high output diesel engines, where high temperature boundary lubrication between the piston ring and the cylinder liner wall surface is critical for successful engine operation. The target temperature focused upon in our research is an operating top ring reversal (TRR) temperature of approximately 538°C. The technology advancement used for this application involves treating porous iron oxide/titanium oxide (Fe2O3/TiO2) and molybdenum (Mo) based composite thermal sprayed coatings with chemical binders to improve coating strength, integrity, and tribological properties. This process dramatically decreases open porosity to form an almost monolithic appearing coating at the surface1.