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A transparent HSDI CI engine was used together with a high speed camera to analyze the liquid phase spray geometry of the fuel types: Swedish environmental class 1 Diesel fuel (MK1), Soy Methyl Ester (B100), n-Heptane (PRF0) and a gas-to-liquid derivate (GTL) with a distillation range similar to B100. The study of the transient liquid-phase spray propagation was performed at gas temperatures and pressures typical for start of injection conditions of a conventional HSDI CI engine. Inert gas was supplied to the transparent engine in order to avoid self-ignition at these cylinder gas conditions. Observed differences in liquid phase spray geometry were correlated to relevant fuel properties. An empirical relation was derived for predicting liquid spray cone angle and length prior to ignition.