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The spray and combustion of diesel fuel were investigated to provide a better understanding of the evaporation and combustion process under the simulated cold-start condition of a diesel engine. The experiment was conducted in a constant volume combustion chamber and the engine cranking period was selected as the target ambient condition. Mie scattering and shadowgraph techniques were used to visualize the liquid- and vapor-phase of the fuel under evaporating non-combustion conditions (oxygen concentration=0%). In-chamber pressure and direct flame visualization were acquired for spray combustion conditions (oxygen concentration=21%). The fuel was injected at an injection pressure of 30 MPa, which is the typical pressure during the cranking period.