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A quantitative and time-resolved technique has been developed to probe the dense spray structure of direct-injection (DI) gasoline sprays in near-nozzle region. This technique uses the line-of-sight absorption of monochromatic x-rays from a synchrotron source to measure the fuel mass with time resolution better than 1 μs. The small scattering cross-section of fuel at x-rays regime allows direct measurements of spray structure that are difficult with most visible-light optical techniques. Appropriate models were developed to determine the fuel density as a function of time.