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An experimental and computational study of the near-wall combustion in a Homogeneous Charge Compression Ignition (HCCI) engine has been conducted by applying laser based diagnostic techniques in combination with numerical modeling. Our major intent was to characterize the combustion in the velocity- and thermal boundary layers. The progress of the combustion was studied by using fuel tracer LIF, the result of which was compared with LDA measurements of the velocity boundary layer along with numerical simulations of the reacting boundary layer. Time resolved images of the PLIF signal were taken and ensemble averaged images were calculated. In the fuel tracer LIF experiments, acetone was seeded into the fuel as a tracer. It is clear from the experiments that a proper set of backgrounds and laser profiles are necessary to resolve the near-wall concentration profiles, even at a qualitative level.