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Mixture formation processes play a vital role on the performance of a D.I. Gasoline engine. Quantitative measurement of liquid and vapor phase concentration distribution in a D.I. gasoline spray is very important in understanding the mixture formation processes. In this paper, an unique laser absorption scattering (LAS) technique was employed to investigate the mixture formation processes of a fuel spray injected by a D.I. gasoline injector into a high pressure and temperature constant volume vessel. P-xylene, which is quite suitable for the application of the LAS technique, was selected as the test fuel. The temporal variations of the concentration distribution of both the liquid and vapor phases in the spray were quantitatively clarified. Then the effects of injection pressure and quantity on the concentration distributions of both the liquid and vapor phases in the spray were analyzed.