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The results of a comprehensive experimental investigation into the exhaust emission performance and combustion properties of neat and blended Gas-To-Liquids (GTL) diesel fuel are presented. A sulphur-free European diesel fuel was used as the reference fuel, and two blends of the GTL diesel fuel with the reference fuel, containing 20% and 50% GTL diesel fuel respectively, were investigated. The study was based on a Mercedes Benz 2.2 liter passenger car diesel engine and presents emission data for both the standard engine calibration settings, as well as settings which were optimized to match the characteristics of each fuel. Vehicle emission tests showed that the GTL diesel fuel results in reductions in HC and CO emissions of greater than 90%, while PM is reduced by 30%, and NOx remains approximately unchanged. Engine bench dynamometer tests showed reductions in soot of between 30% and 60%, and NOx reductions of up to 10% with the GTL diesel fuel, depending on the operating point.