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In the Rankine cycle, the pressure differential generated by the phase change of the working fluid produces turbine output power, which enables the recovery of waste heat from the internal combustion engine. The heat transfer ability of the evaporator is the key factor that determines the quality of turbine's mechanical work. In this paper, the performance of the evaporator with two-phase zone and preheated zone is studied. After obtaining the thermal characteristics of diesel engine exhaust from the experimental data, the mathematical model of the evaporator is built according to the specific working conditions of ORC and geometrical parameters of the evaporator. Three typical engine operating conditions are used to estimate the heat transfer characteristics of the evaporator. The result shows that, in the evaporator, the heat transfer coefficient of the Rankine working fluid is much greater than the exhaust side of the engine.