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In this paper, effect of intake air temperature, coolant temperature, and compression ratio on start of heat release (SOHR) in HCCI engines is investigated. The operational range with HCCI operation was determined experimentally using a CFR (Cooperative Fuels Research) engine with n-butane as the fuel. In-cylinder pressure was processed to evaluate SOHR. The effect of intake air and coolant temperature on SOHR increases as engine speed increases. In order to gain more insight into the combustion phenomena, SOHR was calculated using the theory of Livengood-Wu and compared with the experimental data. Dependence of SOHR on the equivalence ratio shows good correspondence between experiment and calculation. On the contrary, dependence on the intake air temperature and compression ratio shows poorer correspondence with predictions, especially under low engine speed. We interpret this as an indication of the importance of the active intermediate species that remain in the combustion chamber.