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The UBHC emissions during cold starting need to be controlled in order to meet the future stringent standards. This requires a better understanding of the characteristics of the time resolved UBHC signal measured by a high frequency FID and its phasing with respect to the valve events. The computer program supplied with the instrument and currently used to compute the phase shift has many uncertainties due to the unsteady nature of engine operation during starting. A new technique is developed to measure the in-situ phase shift of the UBHC signal under the transient thermodynamic and dynamic conditions of the engine. The UBHC concentration is measured at two locations in the exhaust manifold of one cylinder in a multicylinder port injected gasoline engine. The two locations are 77 mm apart. The downstream probe is positioned opposite to a solenoid-operated injector which delivers a gaseous jet of hydrocarbon-free nitrogen upon command.