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The susceptibility of Advanced High Strength Steels (AHSS) to hydrogen embrittlement (HE) was evaluated on selected high strength sheet steels (DP 600, TRIP 780, TRIP 980, TWIP-Al, TWIP, and Martensitic M220) and the results were compared to data on a lower strength (300 MPa tensile strength) low carbon steel. Tensile samples were cathodically charged and then immediately tensile tested to failure to analyze the mechanical properties of the as-charged steel. The effects of hydrogen on deformation and fracture behavior were evaluated through analysis of tensile properties, necking geometry, and SEM images of fracture surfaces and metallographic samples of deformed tensile specimens. The two fully austenitic TWIP steels were resistant to hydrogen effects in the laboratory charged tensile samples.

Fracture split forged steel connecting rods are utilized in many new high performance automotive engines to increase durability. Higher strength levels are needed as the power density increases. Fracture splitting without plastic deformation is necessary for manufacturability. Metallurgical design is a key for achieving the required performance levels. Several medium carbon steels containing 0.07 wt pct P, 0.06 wt pct S and various amounts of Mn, Si, V, and N were produced by vacuum induction melting laboratory heats and hot working the cast ingots into plates. The plates were cooled at varying rates to simulate typical cooling methods after forging. Microstructures were generally ferrite and pearlite as evaluated by light optical and scanning electron microscopy. Mechanical properties were determined by standard tensile tests, high strain rate notched tensile tests, and Charpy V-notch impact tests to assess “splittability”.

Quenching and partitioning (Q&P) is a novel heat treatment to produce third generation advanced high-strength steels (AHSS). The influence of carbon on mechanical properties of Q&P treated CMnSi-steels was studied using 0.3C-1.5Mn-1.5Si and 0.4C-1.5Mn-1.5Si alloys. Full austenitization followed by two-step Q&P treatments were conducted using varying partitioning times and a fixed partitioning temperature of 400 °C. The results were compared to literature data for 0.2C-1.6Mn-1.6Si, 0.2-3Mn-1.6Si and 0.3-3Mn-1.6Si Q&P treated steels. The comparison showed that increasing the carbon content from 0.2 to 0.4 wt pct increased the ultimate tensile strength by 140 MPa per 0.1 wt pct C up to 1611 MPa without significantly decreasing ductility for the partitioning conditions used. Increased alloy carbon content did not substantially increase the retained austenite fractions. The best combinations of ultimate tensile strength and total elongation were obtained using short partitioning times.

The influence of coatings on fatigue behavior has been examined for the following commercially produced sheet steels: uncoated titanium stabilized interstitial-free (IF); electrogalvanized titanium stabilized IF; hot-dip galvanized aluminum killed, drawing quality (AKDQ); and galvannealed AKDQ. Fully reversed bending fatigue tests were conducted at ambient temperature on Krouse-type flexural fatigue machines. A dependence of crack development was observed and correlated to the microstructure and properties of the different coatings. Furthermore, a functional design relationship for each material was determined through stress-life analysis. The experimentally determined fatigue properties were compared to conventional estimates based on tensile properties which ignore coating effects. The results of this work suggest that ductile coatings may enhance fatigue resistance, while brittle coatings may reduce fatigue life.

With the increased use of tubular steel products, especially for automotive hydroforming applications, there is increased interest in understanding the mechanical properties measured by tensile tests from specimens of different orientations in the tube. In this study, two orientations of tensile specimens were evaluated -- axial specimens with and without flattening and flattened circumferential specimens. Three steels were evaluated -- two thicknesses of aluminum killed drawing quality (AKDQ) steel and one thickness of high strength low alloy (HSLA) steel. Mechanical property data were obtained from the flat stock, conventional production tubes and quasi tubes. Quasi tubes were produced from the flat stock on a 3-roll bender, but the quasi tube was not welded or sized.

The response of HSLA steel, 590R, and dual-phase steel, DP-600, to non-uniform deformation imposed in a laboratory Bending-Under-Tension (BUT) test apparatus was evaluated. Samples were deformed with both low and high back tension forces at bend angles of 45 and 90 degrees, and evaluated to determine the “side-wall curl”, i.e. the curvature in the sheet section in contact with the die. The results indicate that there are no consistent differences between the two steels, 590R and DP-600. It was found that back tension, tensile strength and sheet thickness were the primary factors affecting curl. The bend angle has an influence on curl, with the curl radius at a 90° bend angle being greater than the curl radius at a 45° bend angle.

Quenching & Partitioning (Q&P) is receiving increased attention as a novel Advanced High Strength Steel (AHSS) processing route as promising tensile properties of the “third generation” have been reported. The current contribution reports hole expansion ratios (HER) of Q&P steels and compares the values with HERs obtained for “conventional” AHSS processing routes such as austempering and Quench & Tempering (Q&T). Intercritically annealed C-Mn-Al-Si-P and fully austenitized C-Mn-Si microstructures were studied. Optimum combinations of tensile strength and HER were obtained for fully austenitized C-Mn-Si Q&P samples. Higher HER values were obtained for Q&P than for Q&T steels for similar tempering/partitioning temperatures. Austempering following intercritical annealing results in higher HER than Q&P at similar tensile strength levels. In contrast, Q&P following full austenitization results in higher hole expansion than austempering even at higher strength levels.

Five heats of vanadium-microalloyed steel with carbon contents from 0.29% to 0.40% and sulfur contents from 0.031% to 0.110% were forged into automotive spindles and air cooled. Three of the steels were continuously cast whereas the other two were ingot cast. The forged spindles were subjected to microstructural analysis, mechanical property testing, full component testing and machinability testing. The microstructures of the five steels consisted of pearlite and ferrite which nucleated on prior austenite grain boundaries and predominantly on intragranularly dispersed sulfide inclusions of the resulfurized grades. Ultimate tensile strengths and room temperature Charpy V-notch impact toughness values were relatively insensitive to processing and compositional variations. The room temperature tensile and room-temperature impact properties ranged from 820 MPa to 1000 MPa (120 to 145 ksi) and from 13 Joules to 19 Joules (10 to 14 ft-lbs), respectively, for the various steels.

The influences of laboratory-induced hydrogen on the tensile deformation and fracture behavior of selected sheet steels including conventional DQSK and HSLA steels as well as newer DP and TRIP grades were evaluated. The effects of cold work, simulated paint baking, and natural aging were considered. Hydrogen effects were observable by increased flow stress, decreased ductility, altered neck geometry, and altered fracture mechanisms. Differences among the steels and conditions were observed and interpreted on the basis of microstructure, fracture behavior, and theories of hydrogen embrittlement.

High strain rate sheet tensile tests (up to 300s-1) and Ohio State University (OSU) formability tests (up to an estimated strain rate of 10s-1) were performed to examine the effect of strain rate on the mechanical properties and formability of five ferritic stainless steels: HIGH PERFORMANCE-10™ 409 (HP-10 409), ULTRA FORM® 409 (UF 409), HIGH PERFORMANCE-10™ 439 (HP-10 439), two thicknesses of 18 Cr-Cb™ stainless steel, all supplied by AK Steel, and Duracorr®, a ferrite-tempered martensite dual-phase stainless steel supplied by Bethlehem Steel Corporation. Tensile results show that increasing strain rate resulted in increases in yield stress, flow stress, and stress at instability for all alloys tested. In addition, increases in uniform and total elongation were also found for each of the five alloys.

The effects of subzero treatments on the bending fatigue performance of carburized gear steels were investigated by cantilever bending fatigue testing. Specimens were machined from SAE-4320 and SAE-9310 bar stock steel, gas-carburized, quenched, tempered at 175°C, subzero cooled to -73°C and -196°C, and tempered at 175°C. Bending fatigue specimens were characterized by light metallography to determine microstructure and prior austenite grain size, x-ray diffraction for residual stress and retained austenite contents, microhardness testing, and scanning electron microscopy to evaluate fatigue crack initiation, propagation and overload. Refrigeration treatments caused additional transformation of retained austenite and increased surface hardness and compressive residual stresses. Bending fatigue endurance limits for the SAE-4320 specimens were determined to be 1310 MPa for the as-carburized condition, 1170 MPa for the -73°C condition, and 1280 MPa for the -196°C condition.

The Society of Automotive Engineers Fatigue Design & Evaluation Committee [SAE FD&E] is actively working on a total life project for weldments, in which the welding residual stress is a key contributor to an accurate assessment of fatigue life. Physics-based welding process simulation and various types of residual stress measurements were pursued to provide a representation of the residual stress field at the failure location in the fatigue samples. A well-controlled and documented robotic welding process was used for all sample fabrications to provide accurate inputs for the welding simulations. One destructive (contour method) residual stress measurement and several non-destructive residual stress measurements-surface X-ray diffraction (XRD), energy dispersive X-ray diffraction (EDXRD), and neutron diffraction (ND)-were performed on the same or similarly welded samples.

The strain-induced diffusionless shear transformation of retained austenite to martensite during straining of transformation induced plasticity (TRIP) assisted steels increases strain hardening and delays necking and fracture leading to exceptional ductility and strength, which are attractive for automotive applications. A novel technique that provides the retained austenite volume fraction variation with strain with improved precision is presented. Digital images of the gauge section of tensile specimens were first recorded up to selected plastic strains with a stereo digital image correlation (DIC) system. The austenite volume fraction was measured by synchrotron X-ray diffraction from small squares cut from the gage section. Strain fields in the squares were then computed by localizing the strain measurement to the corresponding region of a given square during DIC post-processing of the images recorded during tensile testing.

In this paper, a two-dimensional microstructure-based finite element modeling method is adopted to investigate the effects of material parameters of the constituent phases on the macroscopic tensile behavior of Q&P steel and to perform a computational material design approach for performance improvement. For this purpose, a model Q&P steel is first produced and various experiments are then performed to characterize the model steel. Actual microstructure-based model is generated based on the information from EBSD, SEM and nano-indentation test, and the material properties for the constituent phases in the model are determined based on the initial constituent properties from HEXRD test and the subsequent calibration of model predictions to tensile test results. The influence of various material parameters of the constituents on the macroscopic behavior is then investigated.

Third generation advanced high strength steels (AHSS) have been developed combining high strength and formability, allowing for lightweighting of vehicle structural components. These AHSS components are exposed to paint baking operations ranging in time and temperature to cure the applied paint. The paint baking treatment, combined with straining induced from part forming, may lead to increased in-service component performance due to a strengthening mechanism known as bake hardening. This study aims to quantify the bake hardening behavior of select AHSS grades. Materials investigated were press hardenable steels (PHS) 1500 and 2000; transformation induced plasticity (TRIP) aided bainitic ferrite (TBF) 1000 and 1200; and dual phase (DP) 1000. The number designations of these grades refer to minimum as-received ultimate tensile strengths in MPa. Paint baking was simulated using industrially relevant times and temperatures from 15 to 60 min and 120 to 200 °C, respectively.