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Concern over health effects associated with diesel exhaust and debate over the influence of high number counts of particles in diesel exhaust prompted research to develop a methodology for diesel particulate matter (PM) characterization. As part of this program, a tractor truck with an electronically managed diesel engine and a dynamometer were installed in the Old Dominion University (ODU) Langley full-scale wind tunnel. This arrangement permitted repeat measurements of diesel exhaust under realistic and reproducible conditions and permitted examination of the steady exhaust plume at multiple points. Background particle size distribution was characterized using a Scanning Mobility Particle Sizer (SMPS). In addition, a remote sampling system consisting of a SMPS, PM filter arrangement, and carbon dioxide (CO2) analyzer, was attached to a roving gantry allowing for exhaust plume sampling in a three dimensional grid. Raw exhaust CO2 levels and truck performance data were also measured.