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It is well-known that gasoline is a poor fuel for HCCI operation due to its high autoignation temperature, while the major problem for diesel HCCI is that the ignition temperature of diesel fuel is too low so that diesel autoignites too early. Interestingly a blend of gasoline and diesel fuel could have desirable characteristics for HCCI operation. The negative valve overlap (NVO) is a practical and feasible control mode for production applications of the HCCI concept. At present, the most serious problem is the difficulty to control the moment of auto-ignition and extend the limited operating window of smooth HCCI operation. In this paper, the promotive effects of diesel fuel on gasoline HCCI combustion were experimentally examined. The diesel fuel as additive was added in advance in different proportion (10% and 20% by mass) into gasoline for the purpose of improving its ignitability. The experiments conducted on a gasoline HCCI engine which was naturally aspirated and unthrottled.