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This work presents the results of an experimental investigation on a GDI injector, in order to analyze fuel injection process and atomization phenomenon, correlating imaging and vibro-acoustic diagnostic techniques. A single-hole, axially-disposed, 0.200 mm diameter GDI injector was used to spray commercial gasoline in a test chamber at room temperature and atmospheric backpressure. The explored injection pressures were ranged from 5.0 to 20.0 MPa. Cycle-resolved acquisitions of the spray evolution were acquired by a high-speed camera. Simultaneously, the vibro-acoustic response of the injector was evaluated. More in detail, noise data acquired by a microphone sensor were analyzed for characterizing the acoustic emission of the injection, while a spherical loudspeaker was used to excite the spray injection at a proper distance detecting possible fuel spray resonance phenomena.