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A novel method is applied to analysis the autoignition phenomenon. Experiments on the study of autoignition characteristics of diesel fuel were carried out with a Controllable Active Thermo-Atmosphere Combustor. The results show that the method for autoignition studying of liquid fuel is of feasibility. Autoignition delay time and autoignition height from the nozzle increase with the coflow temperature decreasing and autoignition delay time changes sensitively under lower coflow temperature. Liftoff height of diesel spray flame decreases with the increasing of coflow temperature. Lower temperature causes higher variance of liftoff height. It might be speculated that there are two different mechanisms of flame stabilization that the lower lift-off heights flames are related to a balance between the flow velocity and flame speed while the higher lift-off heights flames are stabilized by the mixture autoignition.