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The equipment for collecting dilute exhaust samples involves the use of bag materials (i.e., Tedlar®) that emit hydrocarbons that contaminate samples. This study identifies a list of materials and treatments to produce bags that reduce contamination. Based on the average emission rates, baked Tedlar®, Capran® treated with alumina deposition, supercritical CO2 extracted Kynar® and supercritical CO2 extracted Teflon NXT are capable of achieving the target hydrocarbon emission rate of less than 15 ppbC per 30 minutes. CO2 permeation tests were also performed. Tedlar, Capran, Kynar and Teflon NXT showed comparable average permeation rates. Based on the criteria of HC emission performance, changes in measured CO2 concentration, ease of sealing, and ease of surface treatment, none of the four materials could be distinguished from one another.

Particulate and regulated gaseous emissions were characterized in a feasibility study for a 1994 Ford Taurus Flexible Fuel Vehicle (FFV) operating on five fuels. The five fuels included Federal Reformulated Gasoline (RFG); 85% fuel grade methanol and 15% gasoline (M85); 85% denatured ethanol and 15% gasoline (E85d); liquefied petroleum gas (LPG) meeting HD-5 specifications; and industry average compressed natural gas (CNG). The vehicle was operated fuel-rich to simulate a vehicle operating condition leading to increased production of particulate matter. This simulation was accomplished by using a universal exhaust gas oxygen sensor (UEGO) in connection with an external controller. Appropriate aftermarket conversion kits involving closed-loop control and adaptive learning capabilities allowed operation on the gaseous fuels. Particulate emissions were characterized by total mass and particle size.

FTP-UDDS (urban dynamometer driving schedule) exhaust particulate matter (PM) emission rates were determined for 361 light-duty gasoline (LDGV) and 49 diesel passenger vehicles ranging in model year (MY) from 1965 to 1997. LDGVs were recruited into four MY categories. In addition, special effort was made to recruit LDGVs with visible smoke emissions, since these vehicles may be significant contributors to the mobile source PM emission inventory. Both light and heavy-duty diesels where included in the passenger diesel test fleet, which was insufficient in size to separate into the same MY categories as the LDGVs. Vehicles were tested as-received in three areas: Denver, Colorado; San Antonio, Texas; and the South Coast Air Quality Management District, California. The average PM emission rates were 3.3, 79.9, 384 and 558 mg/mi for 1991-97 MY LDGVs, pre-1981 LDGVs, smoking LDGVs and the diesel vehicles, respectively.