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Knocking phenomenon in a spark ignition engine breaks out due to autoignition in the unburned gas region. Investigation on the pre-autoignition reaction, that is, the reaction of cool and blue flames happening before autoignition must be carried out in detail to control knocking. The reactions appear in an extremely short time before autoignition, so, much difficulties accompany an attempt to grasp the situation. In the experiments presented hear, progress situation of pre-autoignition reaction was made clear by visualized phenomena in a rapid compression and expansion machine (R.C.E.M), which had good reproducibility. Taken by two ultra high-speed video cameras. We determined the ignition delay time was caught by analyzing the emission of light from the combustion chamber before knocking occurrence.