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More Mg alloys are being considered for uses in the automotive industry. Since the corrosion performance of Mg alloy components in practical service environments is unknown, long term corrosion testing at automotive proving grounds will be an essential step before Mg alloy components can be implemented in vehicles. However, testing so many Mg alloy candidates for various parts is labor intensive for the corrosion engineers at the proving grounds. This report presents preliminary results in evaluating corrosion performance of Mg alloys based on rapid corrosion and electrochemical tests in the lab. In this study, four Mg alloy candidates for transmission cases and oil pans: AE44, AXJ530, MRI153M and MRI230D were tested in the lab and at General Motors Corporation Milford Proving Ground and their corrosion results were compared.

With the increasing demand for fuel efficient vehicles, technologies like superplastic forming (SPF) are being developed and implemented to allow for the utilization of lightweight automotive sheet materials. While forming under superplastic conditions leads to increased formability in lightweight alloys, such as aluminum, the slower forming times required by the technology can limit the technology to low to mid production levels. One problem that can increase forming time is the reduction of forming pressure due to pressurizing (forming) gas leaks, during the forming cycle, at the die/sheet/blankholder interface. Traditionally, such leaks have been successfully addressed through the use of a seal bead. However, for advanced die technologies that result in reduced cycle times (such as hot draw mechanical performing, which combine aspects of mechanical preforming of the sheet metal followed by SPF), the use of seal beads can restrict the drawing of sheet material into the forming die.

Fatigue behavior of aluminum alloys under multiaxial loading was investigated with both cast aluminum A356-T6 and wrought alloy 6063-T6. The dominant multiaxial fatigue crack preferentially nucleates from flaws like porosity and oxide films located near the free surface of the material. In the absence of the flaws, the cracking/debonding of the second phase particles dominates the crack initiation and propagation. The number of cracked/debonded particles increases with the number of cycles, but the damage rate depends on loading paths. Among various loading paths studied, the circle loading path shows the shortest fatigue life due to the development of complex dislocation substructures and severe stress concentration near grain/cell boundaries and second phase particles.

The impact of texture on r-value and its measurement in magnesium alloy sheets has been studied using digital image correlation and electron backscatter diffraction techniques. Two magnesium alloy sheets with distinct textures were used in the present study, namely, AZ31 with a strong basal texture and ZE21 with a randomized texture. It is well known that a conventionally processed AZ31 magnesium sheet has strong basal texture, necessitating contraction and double twinning to accommodate thinning strain. The strain distribution on the sheet surface evolves nonlinearly with strain, impacting the measured r-value. In particular, the normal approach to measuring r-value based on average strains over the gauge section leads to the erroneous conclusion that r-value increases with deformation. When the r-value is measured locally at any point inside or outside the neck, the r-value is shown to have a constant value of 3 for all strain values.

Due to magnesium alloy's poor weldability, other joining techniques such as laser assisted self-piercing rivet (LSPR) are used for joining magnesium alloys. This research investigates the fatigue performance of LSPR for magnesium alloys including AZ31 and AM60. Tensile-shear and coach peel specimens for AZ31 and AM60 were fabricated and tested for understanding joint fatigue performance. A structural stress - life (S-N) method was used to develop the fatigue parameters from load-life test results. In order to validate this approach, test results from multijoint specimens were compared with the predicted fatigue results of these specimens using the structural stress method. The fatigue results predicted using the structural stress method correlate well with the test results.

Aircraft components are commonly produced with 7000 series aluminum alloys (AA) due to its weight, strength, and fatigue properties. Auto Industry is also choosing more and more aluminum component for weight reduction. Current additive manufacturing (AM) methods fall short of successfully producing 7000 series AA due to the reflective nature of the material along with elements with low vaporization temperature. Moreover, lacking in ideal thermal control, print inherently defective products with such issues as poor surface finish alloying element loss and porosity. All these defects contribute to reduction of mechanical strength. By monitoring plasma with spectroscopic sensors, multiple information such as line intensity, standard deviation, plasma temperature or electron density, and by using different signal processing algorithm, AM defects have been detected and classified.

The effect of temperature and preload on the bolt load retention (BLR) behavior of AZ91D and AE42 magnesium die castings was investigated. The results were compared to those of 380 aluminum die castings. Test temperatures from 125 to 175°C and preloads from 7 to 28 kN were investigated. The loss of preload for AZ91D was more sensitive to temperature than that observed for AE42, especially at low preloads. In general, retained bolt-load was lowest in AZ91D. All test assemblies were preloaded at room temperature and load levels increased when the assemblies reached test temperature. The load-increase was dependent on the preload level, test temperature, alloy, and results from thermal expansion mismatch between the steel bolt and the magnesium alloy components, mitigated by the onset of primary creep. Thermal exposure (aging) of AZ91D at 150°C improved BLR behavior.

Creep-resistant magnesium alloys for automotive powertrain applications offer significant potential for vehicle weight reduction. In this study permanent mold casting, microstructure and creep behavior have been investigated for a series of ternary magnesium alloys (Mg-4Al-4X (X: Ca, Ce, La, Sr) wt%) and AXJ530 (Mg-5Al-3Ca-0.15Sr, wt%). A permanent mold was instrumented with twelve thermocouples and mold temperature was monitored during the casting process. Average mold temperature increased from 200°C to 400°C during a typical alloy casting series (fifteen to twenty castings). The cast microstructure for all alloys consists of primary α-Mg globular phase surrounded by eutectic structure which is composed of intermetallic(s) and α-Mg magnesium phases. The primary cell size of the AXJ530 increased from 18 to 24 μm with increasing mold temperature and a similar trend is expected for all alloys.

Solidification paths and phase stability have been investigated in the creep resistant Mg-Al-Ca based alloys for powertrain applications. The liquidus projection and isothermal sections of the Mg-Al-Ca ternary system were determined, including a ternary (Mg, Al)2Ca intermetallic compound. The solidification of the alloys in the α-Mg primary phase field involves L→α+(Mg, Al)2Ca eutectic reaction in a wide range of compositions and is terminated with invariant reactions that form Mg2Ca or Mg17Al12 phases. The (Mg, Al)2Ca is a high temperature phase and decomposes into Mg2Ca and Al2Ca phases between 773 and 673 K, but the transformation is kinetically quite slow at temperatures below 473 K. Based on this new knowledge, alloy modifications through quaternary elemental additions to improve the solid-solution strength and aging treatments to reinforce the α-Mg phase with precipitates have been demonstrated.

The effects of lubricant on lap shear strength of Spot Friction Welded (SFW) joints made of 6111-T4 alloys were studied. Taguchi L8 design of experiment methodology was used to determine the lubricant effects. The results showed that the lap shear strength increased by 9.9% when the lubricant was present at the top surface compared to that of the baseline (no lubricant) whereas the lap shear strength reduced by 10.2% and 10.9% when the lubricant was present in the middle and at the bottom surfaces compared to that of the baseline (no lubricant), respectively. The microstructure analysis showed a zigzag interface at the joint between the upper and the lower sheet metal for the baseline specimen, the specimens with the lubricant at the top and at the bottom. However, a straight line interface is exhibited at the joint between the upper and the lower sheet for the specimen with the lubricant in the middle. The weld nugget sizes of the lap shear tested specimens were measured.

AZ31B Mg sheet is being considered for automotive applications. This study investigates the effect of pre-treatments, such as heat-treatments and surface treatments, on the corrosion performance of AZ31B sheet, with a goal of learning which pre-treatment can improve corrosion resistance of the sheet material in production. It is found that the heat-treatment and oxidation during a warm and hot forming (WHF) process will not deteriorate the corrosion performance of the AZ31B sheet; polishing and acid etching can clean the surface and significantly increase the corrosion resistance, but corrosion can be accelerated by sandblasting which contaminates the surface. The change in corrosion performance can be associated with surface cleaning or contamination of the sheet by these pre-treatments. Furthermore, the influence of a pre-treatment on the uncoated AZ31B sheet may affect its corrosion behavior after coating.

Magnesium alloys are not corrosion resistant in many applications and they require coating protection. In this study, we developed an electroless E-coating technique for magnesium alloys and discussed a cathodic E-coating deposition mechanism for the electroless E-coating process. This coating can be formed within a few seconds by dipping a magnesium alloy (i.e., AZ91D) in an E-coat bath without applying a current or voltage. The deposited electroless coat can offer good protection to the AZ91D magnesium alloy in 5 wt% NaCl corrosive solution as well as in a phosphating bath. The most interesting finding is that the electroless coating is not sensitive to local damage. No preferential corrosion attack occurred along the scratches made on the coating.

The fundamental relationship between semi-solid processing and microstructure and their effect on the flow characteristics of semi-solid metals have been studied for several years. However, how the process related microstructure influences fatigue properties has not been given the same attention. This study examines the influence of process-related microstructure on the fatigue properties of semi-solid formed A357 alloys. High-solid-fraction (62% solid) and low-solid-fraction (31% and 36% solid) semi-solid formed A357 was tested in axial fatigue with a stress ratio (R) equal to -1. The high solid fraction (HSF) material had better fatigue properties than the low solid fraction (LSF) material. This is attributed to the fatigue crack initiation mechanisms, as related to the fatigue crack initiation features and the strengths of the materials.

The need for improved understanding of new magnesium alloys for the automotive industry continues to grow as the application for these lightweight alloys expands to more demanding environments, particularly in drivetrain components. Their use at elevated temperatures, such as in transmission cases, presents a challenge because magnesium alloys generally have lower creep resistance than aluminum alloys currently employed for such applications. In this study, a new die cast magnesium alloy, MEZ, containing rare earth (RE) elements and zinc as principal alloying constituents, was examined for its bolt-load retention (BLR) properties. Preloads varied from 14 to 28 kN and test temperatures ranged from 125 to 175°C. At all test temperatures and preloads, MEZ retained the greatest fraction of the initial imposed preload when compared to the magnesium alloys AZ91D, AE42, AM50, and the AM50+Ca series alloys.

In this paper the lightweight design and construction of road vehicle aluminum wheels is dealt with, referring particularly to safety. Dedicated experimental tests aimed at assessing the fatigue life behavior of aluminum alloy A356 - T6 have been performed. Cylindrical specimens have been extracted from three different locations in the wheel. Fully reversed strain-controlled and load-controlled fatigue tests have been performed and the stress/strain-life curves on the three areas of the wheel have been computed and compared. The constant amplitude rotary bending fatigue test of the wheel has been simulated by means of Finite Element method. The FE model has been validated by measuring the strain at several points of the wheel during the actual test. From the FE model, the stress tensor time history on the whole wheel over a loading cycle has been extracted.

Quantification of residual stresses is an important engineering problem impacting manufacturabilty and durability of metallic components. An area of particular concern is residual stresses that can develop during heat treatment of metallic components. Many heat treatments, especially in heat treatable cast aluminum alloys, involve a water-quenching step immediately after a solution-treatment cycle. This rapid water quench has the potential to induce high residual stresses in regions of the castings that experience large thermal gradients. These stresses may be partially relaxed during the aging portion of the heat treatment. The goal of this research was to develop a test sample and quench technique to quantify the stresses created by steep thermal gradients during rapid quenching of cast aluminum. The development and relaxation of residual stresses during the aging cycle was studied experimentally with the use of strain gauges.

New high-temperature Mg alloys are being considered to replace 380 Al in transmission cases, wherein bolt-load retention, and creep, is of prime concern. One of these alloys is die cast AE42, which has much better creep properties than does AZ91D but is still not as creep resistant as 380 Al. It is thus important to investigate bolt-load retention and creep of AE42 as an initial step in assessing its suitability as a material for transmission housings. To that end, the bolt-load retention behavior of die-cast AE42, AZ91D and 380 Al have been examined using standard M10 bolts specially instrumented with stable high-temperature strain gages. The bolt-load retention test pieces were die cast in geometries approximating the flange and boss regions in typical bolted joints. Bolt-load retention properties were examined as a function of time (at least 100 hours), temperature (150 and 175 °C) and initial bolt preload (14 to 34 kN).

In this paper, a microstructure-based three-dimensional (3D) finite element modeling method is adopted to investigate the effects of porosity in thin-walled high pressure die-cast (HPDC) magnesium alloys on their ductility. For this purpose, the cross-sections of AM60 casting samples are first examined using optical microscope and X-ray tomography to obtain the general information on the pore distribution features. The experimentally observed pore distribution features are then used to generate a series of synthetic microstructure-based 3D finite element models with different pore volume fractions and pore distribution features. Shear and ductile damage models are adopted in the finite element analyses to induce the fracture by element removal, leading to the prediction of ductility.

Compositional and microstructural variations in a casting can often result in rather significant variations in the response to a given aging treatment, leading to location dependent mechanical properties. The objective of this study is to determine the effect of copper content and solidification rate on the aging behavior of a type 319 cast aluminum alloy. The nominal composition of the alloy is Al-7% Si-3.5% Cu-0.25% Mg, however, typical secondary 319 aluminum specifications allow copper levels to vary from 3-4%. Solidification rates throughout a casting can vary greatly due to, among other factors, differences in section size. To determine the effect of copper level and solidification rate on the aging response, aging curves were experimentally developed for this alloy. Three different copper levels (3, 3.5, 4%) and two solidification rates were used for this study. Aging temperatures ranged from 150-290°C with nine aging times at each temperature.

The use of die cast magnesium for automobile transmission cases offers promise for reducing weight and improving fuel economy. However, the inferior creep resistance of magnesium alloys at high temperature is of concern since transmission cases are typically assembled and joined by pre-loaded bolts. The stress relaxation of the material could thus adversely impact the sealing of the joint. One means of assessing the structural integrity of magnesium transmission cases is modeling the bolted joint, the topic of this paper. The commercial finite element code, ABAQUS, was used to simulate a well characterized bolt joint sample. The geometry was simulated with axi-symmetric elements with the exact geometry of a M10 screw. Frictional contact between the male and female parts is modeled by using interface elements. Material creep is described by a time hardening power law whose parameters are fit to experimental creep test data.