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The increased severity and prevalence of insoluble deposits formed on fuel injectors in gasoline direct injection (GDI) engines precipitates negative environmental, economic and healthcare impacts. A necessary step in mitigating deposits is to unravel the molecular compositions of these complex layered materials. But very little molecular data has been acquired. Mass spectrometry shows promise but most techniques require the use of solvents, making them unsuited for analyzing insoluble deposits. Here, we apply the high mass-resolving power and in-situ analysis capabilities of 3D OrbitrapTM secondary ion mass spectrometry (3D OrbiSIMS) to characterize deposits formed on the external tip and internal needle from a GDI injector. This is the first application of the technique to study internal GDI deposits. Polycyclic aromatic hydrocarbons (PAHs) are present up to higher maximum masses in the external deposit.

The determination of size distribution of soot particles and agglomerates in oil samples using a Nanosight LM14 to perform Nanoparticle Tracking Analysis (NTA) is described. This is the first application of the technique to sizing soot-in-oil agglomerates and offers the advantages of relatively high rates of sample analysis and low cost compared to Transmission Electron Microscopy (TEM). Lubricating oil samples were drawn from the sump of automotive diesel engines run under a mix of light duty operating conditions. The oil samples were diluted with heptane before analysing. Results from NTA analysis were compared with the outputs of a more conventional analysis based on Dynamic Light Scattering (DLS). This work shows that soot-in-oil exists as agglomerates with average size of 115 nm. This is also in good agreement with TEM analysis carried out in a previous work. NTA can measure soot particles in polydisperse oil solutions and report the size distribution of soot-in-oil aggregates.

The oil distribution system of an automotive light duty engine typically has an oil pump mechanically driven through the front-endancillaries-drive or directly off the crankshaft. Delivery pressure is regulated by a relief valve to provide an oil gallery pressure of typically 3 to 4 bar absolute at fully-warm engine running conditions. Electrification of the oil pump drive is one way to decouple pump delivery from engine speed, but this does not alter the flow distribution between parts of the engine requiring lubrication. Here, the behaviour and benefits of a system with an electrically driven, fixed displacement pump and a distributor providing control over flow to crankshaft main bearings and big end bearings is examined. The aim has been to demonstrate that by controlling flow to these bearings, without changing flow to other parts of the engine, significant reductions in engine friction can be achieved.

The size and morphology of soot particles and agglomerates extracted from lubricating oil drawn from the sump of a diesel engine have been investigated and compared using Transmission Electron Microscopy (TEM) and Nanoparticle Tracking Analysis (NTA). Samples were prepared for electron microscopy imaging by both centrifugation and solvent extraction to investigate the impact of these procedures on the morphological characteristics, such as skeleton length and width and circularity, of the obtained soot. It was shown that centrifugation increases the extent of agglomeration within the sample, with 15% of the agglomerates above 200 nm compared to only 11% in the solvent extracted soot. It was also observed that the width of centrifugation extracted soot was typically 10 nm to 20 nm larger than that of solvent extracted soot, suggesting that centrifugation forces the individual agglomerate chains together.

A computational model has been developed to support investigations of temperature, heat flow and friction characteristics, particularly in connection with warm-up behaviour. A lumped capacity model of the engine block and head, empirically derived correlations for local heat transfer and friction losses, and oil and coolant circuit descriptions form the core of the model. Validation of the model and illustrative results are reported.

Two methods of determining the rate of heat transfer from the combustion chamber have been investigated. A First Law analysis is shown to be ill-conditioned because of sensitivity to heat release and gas property calculations. An alternative approach equates cycle-averaged chamber heat transfer to the difference between heat rejected to the coolant and gas heat transfer to the exhaust port. This has been examined as a basis for calibrating the Woschni correlation.

The rate of heat rejection to the coolant system of an internal combustion engine depends upon coolant composition, among other factors, because this influences the coolant side heat transfer coefficient. The correlation developed by Taylor and Toong for heat transfer rate has been modified to account for this effect. The modification retains the gas-to-coolant passage thermal resistance implicit in the original correlation. The modified correlation gives predictions in agreement with experimental data. Compared to 100% water, mixtures of 50% ethylene glycol/50% water lower heat rejection rates by typically 5% and up to 25% in the extreme. This depends upon local conditions in the coolant circuit, which can give rise to different heat transfer regimes. Application of the modified correlation is outlined and illustrated.

A correlation for total gas-side heat transfer rate has been derived from the analysis of engine data for measured heat rejection rate, frictional dissipation, and published data on exhaust port heat transfer. The correlation is related to the form developed by Taylor and Toong, and the analysis draws on this. However, cylinder and exhaust port contributions are separated. Two empirical constants are fixed to best match predicted to measured results for heat rejection to coolant and oil cooler under steady-state conditions, and also for exhaust port heat transfer rates. The separated contributions also defined a correlation for exhaust port heat transfer rate. The description of gas-side heat transfer is suited to needs for the analysis of global thermal behaviour of engines.

The thermal efficiency of an internal combustion engine at steady state temperatures is typically in the region of 25-35%[1]. In a cold start situation, this reduces to be between 10% and 20% [2]. A significant contributor to the reduced efficiency is poor performance by the engine lubricant. Sub optimal viscosity resulting from cold temperatures leads to poor lubrication and a subsequent increase in friction and fuel consumption. Typically, the engine lubricant takes approximately twenty minutes [3] to reach steady state temperatures. Therefore, if the lubricant can reach its steady state operating temperature sooner, the engine's thermal efficiency will be improved. It is hypothesised that, by decoupling the lubricant from the thermal mass of the surrounding engine architecture, it is possible to reduce the thermal energy loss from the lubricant to the surrounding metal structure in the initial stages of warm-up.

Characterization of soot nanoparticle morphology can be used to develop understanding of nanoparticle interaction with engine lubricant oil and its additives. It can be used to help direct modelling of soot-induced thickening, and in a more general sense for combatting reductions in engine efficiency that occur with soot-laden oils. Traditional 2D transmission electron microscopy (TEM) characterization possesses several important shortcomings related to accuracy that have prompted development of an alternative 3D characterization technique utilizing electron tomography, known as 3D-TEM. This work details progress made towards facilitating semi-automated image acquisition and processing for location of structures of interest on the TEM grid. Samples were taken from a four cylinder 1.4 L gasoline turbocharged direct injection (GTDI) engine operated in typically extra-urban driving conditions for 20,284 km, with automatic cylinder deactivation enabled.

The influence of size and concentration of carbon nanoparticle on the viscosity of an SAE 5W-30 lubricant oil has been investigated experimentally. Data were collected for oil samples drawn from sump of light duty automotive diesel engines. The average size of soot particles in the used oil samples was in the range of 180-320nm with concentrations ranging from 0 to 2 percentage by weight (wt. %.). A Brookfield DV-II Pro rotary viscometer was used to measure dynamic viscosity at low shear rates and temperatures of 40°C and 90°C. Nanoparticle concentration and particle size distribution were evaluated using Thermo-Gravimetric Analysis (TGA) and Dynamic Light Scattering (DLS) respectively. The viscosity of suspensions of graphite powder in lubricant oil was also investigated for concentrations ranging from 0 to 2 wt. %. The results show that dynamic viscosity increases with increasing soot content and decreasing temperature.

The dilution of lubricating oil by fuel has adverse effects on engine wear, oil lubricity, air/fuel ratio control and feedgas emissions. Dilution is one of the factors limiting oil change intervals. The level and rate of accumulation depend on engine operating conditions and patterns of vehicle use. The work reported here develops and evaluates an empirical model to predict accumulation characteristics. This is aligned to requirements for predictions of dilution build-up in service. Predictions are shown to be in good agreement with data given in the literature. The model is used to investigate the influence of patterns of vehicle use on dilution.