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Technical Paper

Effects of Lubricating Oil Metallic Content on Morphology, Nanostructure and Graphitization Degree of Diesel Engine Exhaust Particles

In this paper, the influences of metallic content of lubricating oils on diesel particles were investigated. Three lubricating oils with different levels of metallic content were used in a 2.22 Liter, two cylinders, four stroke, and direct injection diesel engine. 4.0 wt. % and 8 wt. % antioxidant and corrosion inhibitor (T202) were added into baseline lubricating oil to improve the performance respectively. Primary particle diameter distributions and particle nanostructure were compared and analyzed by Transmission Electron Microscope. The graphitization degrees of diesel particles from different lubricating oils were analyzed by Raman spectroscopy. Conclusions drawn from the experiments indicate that the metallic content increases the primary particles diameter at 1600 rpm and 2200 rpm. The primary particles diameter ranges from 5 nm to 65 nm and the distribution conformed to Gaussian distribution.
Technical Paper

Effect of Ashless Dispersant on the Morphology, Size, Nanostructure and Graphitization Degree of Diesel Exhaust Particles

The aim of this research is to investigate the effects of ashless dispersant of lube oils on diesel exhaust particles. Emphasis is placed on particle size, morphology, nanostructure and graphitization degree. Three kinds of lube oils with different percentages of ashless dispersant were used in a two-cylinder diesel engine. Ashless dispersant (T154), which is widely used in petrochemical industry, were added into baseline oil at different blend percentages (4.0% and 8.0% by weight) to improve lubrication and cleaning performance. A high resolution Transmission Electron Microscope (HRTEM) and a Raman spectroscopy were employed to analyze and compare particle characteristics. According to the experiment results, primary particles diameter ranges from 3 nm to 65 nm, and the diameter distribution conformed to Gaussian distribution. When the ashless dispersant was used, the primary particles diameter decrease obviously at both 1600 rpm and 2200 rpm.