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In this paper, the influences of metallic content of lubricating oils on diesel particles were investigated. Three lubricating oils with different levels of metallic content were used in a 2.22 Liter, two cylinders, four stroke, and direct injection diesel engine. 4.0 wt. % and 8 wt. % antioxidant and corrosion inhibitor (T202) were added into baseline lubricating oil to improve the performance respectively. Primary particle diameter distributions and particle nanostructure were compared and analyzed by Transmission Electron Microscope. The graphitization degrees of diesel particles from different lubricating oils were analyzed by Raman spectroscopy. Conclusions drawn from the experiments indicate that the metallic content increases the primary particles diameter at 1600 rpm and 2200 rpm. The primary particles diameter ranges from 5 nm to 65 nm and the distribution conformed to Gaussian distribution.