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Behavior of sprays formed by slit nozzle as well as swirl nozzles with the spray cone angle in the range of 40° ∼110 ° were studied in a constant volume N2 gas chamber. The fuels used are iso-pentane, n-heptane, benzene and gasoline. The ambient pressure and temperature were raised up to 1.0 MPa and 465 K, respectively. The injection pressure was mainly set at 8 MPa. Spray penetrates at an almost constant speed for a while after injection start and begins to decelerate at a certain point. This point was judged as breakup point, based on a momentum theory on spray motion, the observation of spray inside and the analysis of the spray front reacceleration which occurs under highly volatile condition.