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Because niobium-clad 304L stainless steel sheets are considered for use as bipolar plates in polymer electrolyte membrane (PEM) fuel cells, their mechanical behavior and failure mechanism are important to be examined. As-rolled and annealed specimens were tested in tension, bending and flattening. The effects of annealing temperature and time on the mechanical behavior and failure mechanism were investigated. Micrographic analyses of bent and flattened specimens showed that the as-rolled specimens have limited ductility and that the annealed specimens can develop an intermetallic layer of thickness of a few microns. The annealed specimens failed due to the breakage of intermetallic layer causing localized necking and the subsequent failure of Nb layer. The springback angles of the as-rolled and annealed specimens were also obtained from guided-bend tests.

With the increasing demand for fuel efficient vehicles, technologies like superplastic forming (SPF) are being developed and implemented to allow for the utilization of lightweight automotive sheet materials. While forming under superplastic conditions leads to increased formability in lightweight alloys, such as aluminum, the slower forming times required by the technology can limit the technology to low to mid production levels. One problem that can increase forming time is the reduction of forming pressure due to pressurizing (forming) gas leaks, during the forming cycle, at the die/sheet/blankholder interface. Traditionally, such leaks have been successfully addressed through the use of a seal bead. However, for advanced die technologies that result in reduced cycle times (such as hot draw mechanical performing, which combine aspects of mechanical preforming of the sheet metal followed by SPF), the use of seal beads can restrict the drawing of sheet material into the forming die.

Due to magnesium alloy's poor weldability, other joining techniques such as laser assisted self-piercing rivet (LSPR) are used for joining magnesium alloys. This research investigates the fatigue performance of LSPR for magnesium alloys including AZ31 and AM60. Tensile-shear and coach peel specimens for AZ31 and AM60 were fabricated and tested for understanding joint fatigue performance. A structural stress - life (S-N) method was used to develop the fatigue parameters from load-life test results. In order to validate this approach, test results from multijoint specimens were compared with the predicted fatigue results of these specimens using the structural stress method. The fatigue results predicted using the structural stress method correlate well with the test results.

In this paper, failure modes of dissimilar laser welds in lap-shear specimens of low carbon steel and high strength low alloy (HSLA) steel sheets are investigated based on experimental observations. Micro-hardness tests across the weld zones of dissimilar laser welds were conducted. The hardness values of the fusion zones and heat affected zones are significantly higher than those of the base metals. The fatigue lives and the corresponding failure modes of laser welds as functions of the load ranges are then examined. Optical micrographs of the laser welds before and after failure under quasi-static and cyclic loading conditions are then examined. The failure modes and fatigue behaviors of the laser welds under different loading conditions are different. Under quasi-static loading conditions, a necking failure occurred in the upper low carbon steel sheet far away from the laser weld.

In this paper, the analytical stress intensity factor and J integral solutions for welds in lap-shear specimens of two dissimilar sheets based on the beam bending theory are first reviewed. The solutions are then presented in the normalized forms. Next, two-dimensional finite element analyses were selectively conducted to validate the analytical solutions based on the beam bending theory. The interface crack parameters, the stress intensity factor solutions, and the J integral solutions for welds in lap-shear specimens of different combinations of steel, aluminum, and magnesium, and the combination of aluminum and copper sheets of different thickness ratios are then presented for convenient fracture and fatigue analyses. The transition thickness ratios for critical crack locations for different combinations of dissimilar materials are then determined from the analytical solutions.

The evolution of microstructure in a Mg 3.4%AI-0.16%Zn-0.33%Mn alloy tube was studied during deformation by ring hoop tension testing (RHTT). When the tests were carried out at moderate temperatures and relatively high strain rates, the accompanying c-axis strains were mainly accommodated by twin formation. At temperatures above 200°C and the lowest strain rate (0.001s-1), the formation of voids in the partially dynamically recrystallized regions caused premature fracture. The microstructural development in hot gasformed samples was similar to that observed during RHTT testing. These results indicate that RHTT testing is an effective way of studying the deformation behavior of Mg alloys during tube gas forming.

Aircraft components are commonly produced with 7000 series aluminum alloys (AA) due to its weight, strength, and fatigue properties. Auto Industry is also choosing more and more aluminum component for weight reduction. Current additive manufacturing (AM) methods fall short of successfully producing 7000 series AA due to the reflective nature of the material along with elements with low vaporization temperature. Moreover, lacking in ideal thermal control, print inherently defective products with such issues as poor surface finish alloying element loss and porosity. All these defects contribute to reduction of mechanical strength. By monitoring plasma with spectroscopic sensors, multiple information such as line intensity, standard deviation, plasma temperature or electron density, and by using different signal processing algorithm, AM defects have been detected and classified.

The effect of temperature and preload on the bolt load retention (BLR) behavior of AZ91D and AE42 magnesium die castings was investigated. The results were compared to those of 380 aluminum die castings. Test temperatures from 125 to 175°C and preloads from 7 to 28 kN were investigated. The loss of preload for AZ91D was more sensitive to temperature than that observed for AE42, especially at low preloads. In general, retained bolt-load was lowest in AZ91D. All test assemblies were preloaded at room temperature and load levels increased when the assemblies reached test temperature. The load-increase was dependent on the preload level, test temperature, alloy, and results from thermal expansion mismatch between the steel bolt and the magnesium alloy components, mitigated by the onset of primary creep. Thermal exposure (aging) of AZ91D at 150°C improved BLR behavior.

Creep-resistant magnesium alloys for automotive powertrain applications offer significant potential for vehicle weight reduction. In this study permanent mold casting, microstructure and creep behavior have been investigated for a series of ternary magnesium alloys (Mg-4Al-4X (X: Ca, Ce, La, Sr) wt%) and AXJ530 (Mg-5Al-3Ca-0.15Sr, wt%). A permanent mold was instrumented with twelve thermocouples and mold temperature was monitored during the casting process. Average mold temperature increased from 200°C to 400°C during a typical alloy casting series (fifteen to twenty castings). The cast microstructure for all alloys consists of primary α-Mg globular phase surrounded by eutectic structure which is composed of intermetallic(s) and α-Mg magnesium phases. The primary cell size of the AXJ530 increased from 18 to 24 μm with increasing mold temperature and a similar trend is expected for all alloys.

Solidification paths and phase stability have been investigated in the creep resistant Mg-Al-Ca based alloys for powertrain applications. The liquidus projection and isothermal sections of the Mg-Al-Ca ternary system were determined, including a ternary (Mg, Al)2Ca intermetallic compound. The solidification of the alloys in the α-Mg primary phase field involves L→α+(Mg, Al)2Ca eutectic reaction in a wide range of compositions and is terminated with invariant reactions that form Mg2Ca or Mg17Al12 phases. The (Mg, Al)2Ca is a high temperature phase and decomposes into Mg2Ca and Al2Ca phases between 773 and 673 K, but the transformation is kinetically quite slow at temperatures below 473 K. Based on this new knowledge, alloy modifications through quaternary elemental additions to improve the solid-solution strength and aging treatments to reinforce the α-Mg phase with precipitates have been demonstrated.

The effects of lubricant on lap shear strength of Spot Friction Welded (SFW) joints made of 6111-T4 alloys were studied. Taguchi L8 design of experiment methodology was used to determine the lubricant effects. The results showed that the lap shear strength increased by 9.9% when the lubricant was present at the top surface compared to that of the baseline (no lubricant) whereas the lap shear strength reduced by 10.2% and 10.9% when the lubricant was present in the middle and at the bottom surfaces compared to that of the baseline (no lubricant), respectively. The microstructure analysis showed a zigzag interface at the joint between the upper and the lower sheet metal for the baseline specimen, the specimens with the lubricant at the top and at the bottom. However, a straight line interface is exhibited at the joint between the upper and the lower sheet for the specimen with the lubricant in the middle. The weld nugget sizes of the lap shear tested specimens were measured.

Thermal distortions of friction disks caused by frictional heating modify pressure distribution on friction surfaces. Pressure distribution, in turn, determines distribution of generated frictional heat. These interdependencies create a complex thermoelastic system that, under some conditions, may become unstable and may lead to severe pressure concentrations with very high local temperature and stress. The phenomenon is responsible for many common thermal failure modes of friction elements and is known as frictionally excited thermoelastic instability (TEI). In the paper, one of the cases of TEI is investigated theoretically and experimentally. The study involves a two-disk structure with one fiction disk and one matching steel disk that have one friction interface. An unsteady heat conduction problem and an elastic contact problem are modeled as axisymmetric ones and are solved using the finite element method.

Federal standards that mandate improved fuel economy have resulted in the increased use of lightweight materials in automotive applications. However, the environmental burdens associated with a product extend well beyond the use phase. Life cycle assessment is the science of determining the environmental burdens associated with the entire life cycle of a given product from cradle-to-grave. This report documents the environmental burdens associated with every phase of the life cycle of two fuel tanks utilized in full-sized 1996 GM vans. These vans are manufactured in two configurations, one which utilizes a steel fuel tank, and the other a multi-layered plastic fuel tank consisting primarily of high density polyethylene (HDPE). This study was a collaborative effort between GM and the University of Michigan's National Pollution Prevention Center, which received funding from EPA's National Risk Management Research Laboratory.

The fundamental relationship between semi-solid processing and microstructure and their effect on the flow characteristics of semi-solid metals have been studied for several years. However, how the process related microstructure influences fatigue properties has not been given the same attention. This study examines the influence of process-related microstructure on the fatigue properties of semi-solid formed A357 alloys. High-solid-fraction (62% solid) and low-solid-fraction (31% and 36% solid) semi-solid formed A357 was tested in axial fatigue with a stress ratio (R) equal to -1. The high solid fraction (HSF) material had better fatigue properties than the low solid fraction (LSF) material. This is attributed to the fatigue crack initiation mechanisms, as related to the fatigue crack initiation features and the strengths of the materials.

This paper describes the tensile creep and microstructure of Mg-Al-Ca-based ACX magnesium alloys being developed for powertrain applications. Important creep parameters, i.e., secondary creep rate and creep strength, for the new alloys are reported. Tensile creep properties of the newly developed ACX alloys are significantly better than those of AE42 alloy, which is the benchmark creep-resistant magnesium die casting alloy. Creep mechanisms for different temperature/stress regimes are proposed. A new intermetallic phase, (Mg,Al)2Ca, was identified in the microstructure of the ACX alloys, and is proposed to be responsible for the improved creep resistance of the alloys.

The need for improved understanding of new magnesium alloys for the automotive industry continues to grow as the application for these lightweight alloys expands to more demanding environments, particularly in drivetrain components. Their use at elevated temperatures, such as in transmission cases, presents a challenge because magnesium alloys generally have lower creep resistance than aluminum alloys currently employed for such applications. In this study, a new die cast magnesium alloy, MEZ, containing rare earth (RE) elements and zinc as principal alloying constituents, was examined for its bolt-load retention (BLR) properties. Preloads varied from 14 to 28 kN and test temperatures ranged from 125 to 175°C. At all test temperatures and preloads, MEZ retained the greatest fraction of the initial imposed preload when compared to the magnesium alloys AZ91D, AE42, AM50, and the AM50+Ca series alloys.

A fastener finish quality monitor based on electrochemical impedance spectroscopy (EIS) has been successfully demonstrated on coated steel fasteners. The coating qualities can be assessed by comparing the measured spectrum with stored spectra of known samples, or by determining values of the coating-specific parameters extracted from the spectrum. Three areas of applications have been identified: (1). Quality control in the plant, (2). Coating process development, and (3). Accelerated corrosion evaluation.

Quantification of residual stresses is an important engineering problem impacting manufacturabilty and durability of metallic components. An area of particular concern is residual stresses that can develop during heat treatment of metallic components. Many heat treatments, especially in heat treatable cast aluminum alloys, involve a water-quenching step immediately after a solution-treatment cycle. This rapid water quench has the potential to induce high residual stresses in regions of the castings that experience large thermal gradients. These stresses may be partially relaxed during the aging portion of the heat treatment. The goal of this research was to develop a test sample and quench technique to quantify the stresses created by steep thermal gradients during rapid quenching of cast aluminum. The development and relaxation of residual stresses during the aging cycle was studied experimentally with the use of strain gauges.

New high-temperature Mg alloys are being considered to replace 380 Al in transmission cases, wherein bolt-load retention, and creep, is of prime concern. One of these alloys is die cast AE42, which has much better creep properties than does AZ91D but is still not as creep resistant as 380 Al. It is thus important to investigate bolt-load retention and creep of AE42 as an initial step in assessing its suitability as a material for transmission housings. To that end, the bolt-load retention behavior of die-cast AE42, AZ91D and 380 Al have been examined using standard M10 bolts specially instrumented with stable high-temperature strain gages. The bolt-load retention test pieces were die cast in geometries approximating the flange and boss regions in typical bolted joints. Bolt-load retention properties were examined as a function of time (at least 100 hours), temperature (150 and 175 °C) and initial bolt preload (14 to 34 kN).

In this paper, a microstructure-based three-dimensional (3D) finite element modeling method is adopted to investigate the effects of porosity in thin-walled high pressure die-cast (HPDC) magnesium alloys on their ductility. For this purpose, the cross-sections of AM60 casting samples are first examined using optical microscope and X-ray tomography to obtain the general information on the pore distribution features. The experimentally observed pore distribution features are then used to generate a series of synthetic microstructure-based 3D finite element models with different pore volume fractions and pore distribution features. Shear and ductile damage models are adopted in the finite element analyses to induce the fracture by element removal, leading to the prediction of ductility.