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The selection of parameters during friction stir spot welding of Al-alloys and Mg-alloys is discussed. The role of tool rotation speed, plunge rate, and dwell time is examined in relation to the tool heating rate,temperature, force, and torque that occur during spot welding. In order to reduce the cycle time and tool force during Al- alloy spot welding, it is necessary to increase the tool rotation speed >1500 RPM. The measured peak temperature in the stir zone is determined by the rotation speed and dwell time, and is ultimately limited by the solidus of the alloy. When tool rotation speeds >1500 RPM are employed during AZ91 Mg-alloy spot welding, the tendency for melted film formation and cracking are greatly increased.

A novel processing method for fabricating high porosity microcellular ceramic foams for sound absorption applications has been developed. The strategy for fabricating the ceramic foams involves: (i) forming some shapes using a mixture of preceramic polymer and expandable microspheres by a conventional ceramic forming method, (ii) foaming the compact by heating, (iii) cross-linking the foamed body, and (iv) transforming the foamed body into ceramic foams by pyrolysis. By controlling the microsphere content and that of the base elastomer, it was possible to adjust the porosity with a very high open-cell content (ranging between 43 - 95%), high microcellular cell densities (9 × 108 - 1.6 × 109 cells/cm3) and desired expansion ratios (3 - 6 folds). Sound absorption testing has been performed using ASTM C-384 standard test. The preliminary results show that ceramic foams are candidate sound absorption materials.

Friction stir spot welding of Mg-alloy AZ91 is investigated. The temperature cycles within the stir zone and in the TMAZ region are examined using thermocouples, which are located within the tool itself and also by locating thermocouples in drilled holes at specific locations relative to the bottom of the tool shoulder and the periphery of the rotating pin. The measured temperatures in the stir zone range from 437°C to 460°C (0.98Ts, where Ts is the solidus temperature in degrees Kelvin) in AZ91 spot welds produced using plunge rates from 2.5 and 25 mm/s. The thermal cycle within the stir zone formed during AZ91 spot welding could not be measured by locating thermocouples within the workpiece in drilled holes adjacent to the periphery of the rotating pin.

Eco-efficient and cost effective natural fibre - thermoplastic composites have gained attention to a great extent in the automotive industry. Most of the OEM specifications for automotive interior parts, for example, instrument panels, recommend the composite should have a minimum flexural modulus of 1900 MPa, a notched Impact strength greater than 150 J/m at room temperature and a melt flow index of 5 g/10min and above [1, 2 and 3]. The objective of this work was to develop a high performance hybrid composite by injection molding process of the composites made from natural fibre in combination with glass fibre or calcium carbonate in a thermoplastic matrix to meet the specifications required for automotive interior parts applications. Mechanical properties, such as tensile and flexural strengths and moduli of the composites prepared, were found to be highly promising.

In this work hemp fibers were chemically treated in order to improve the fiber/matrix interaction in hemp fiber/unsaturated polyester composites prepared by a Resin Transfer Molding (RTM) process. Chemicals used for paper sizing (AKD, ASA, Rosin Acid and SMA) as well as a silane compound and sodium hydroxide were used to modify the fibers' surface. The tensile, flexural and impact properties of the resulting materials were measured. A slight improvement in mechanical properties was observed for the SMA, silane and alkali treated specimens. However close analysis of these tests and of the fracture surface of the samples showed that there was no amelioration of the fiber/matrix adhesion. It was found that predicted tensile strengths using the rule of mixture were very close to the experimental values obtained in this work. Finally the properties of an hybrid glass fiber/hemp fiber composite were found to be very promising

Energy generation and utilization during friction stir spot welding of Al 6061-T6 and AM50 sheet materials are investigated. The dimensions of the stir zones during plunge testing are largely unchanged when the tool rotational speed increases from 1500 RPM to 3000 RPM (for a plunge rate of 1 mm/s) and when the rate of tool penetration increases from 1 mm/s to 10 mm/s (for a tool rotational speed of 3000 RPM). The energy resulting from tool rotation is also unaffected when higher tool rotational speeds are applied. The rotating pin accounts for around 70% and 66% of the energy generated when 6.3 mm thick Al 6061-T6 and AM50 sheet materials are spot welded without the application of a dwell period. In direct contrast, the contribution made by the tool shoulder increases to around 48% (Al 6061-T6) and to 65% (AM50) when a four second long dwell period is incorporated during spot welding of 6.3 mm thick sheets.

TPO is being used to make automotive parts for its number of advantages: i) low temperature flexibility and ductility, ii) excellent impact/stiffness/flow balance, iii) excellent weatherability, and iv) free-flowing pellet form for easy processing, storage, and handling. However, by foaming TPO, due to its higher rigidity-to-weigh ratio, it would offer additional advantages over the solid counterparts in terms of reduced weight, reduced material cost, and decreased fuel usage without compromising their performance. Since a major component in TPO is polypropylene (PP), understanding PP foaming behaviours is an important step towards understanding TPO foaming. For foam materials, cell density and cell size are two significant parameters that affect their material properties. In this research, we observed the cell nucleation and initial growth behaviours of PP foams blown with CO2 under various experimental conditions in a batch foaming simulation system.

Foaming of a thermoplastic polyolefin (TPO) is gaining interests because of its superior mechanical properties of foamed automotive parts, such as lightweight and high performance to weight ratio, etc. In this context, understanding of the thermophysical properties of PP/gas and TPO/gas mixtures is critically important. This paper will present the newly developed experimental technique to accurately measure the swelling of PP and TPO due to gas dissolution at elevated temperatures and pressures. Our technique measures the geometry of the pendent drop accurately from the captured images to obtain the volume swelling data. It determines the boundary location of the polymer/gas sample accurately by magnifying the sample drop locally along its edge before capturing the image. The automated high-precision XY stage is chosen as the platform to control the motion of the CCD camera.

This work is based on a process to develop novel cellulose microfibre reinforced composite materials, and to understand fundamental mechanical properties of these composites. Cellulose microfibres having diameters <1 μm were generated from bleached kraft pulp by a combination of high shear refining and subsequent cryocrushing under liquid nitrogen, followed by filtration through a 60 mesh screen. Through film casting in polyvinyl alcohol, theoretical stiffness of the microfibres was calculated as 69 GPa. Subsequently, these microfibres were successfully dispersed in the bioplastics thermoplastic starch and polylactic acid (PLA), using conventional processing equipments. The high aspect ratio of these microfibres coupled with their high tensile properties imparted superior mechanical strength and stiffness to the composites. These indicated that by suitably choosing the polymer, excellent reinforcement can be achieved for high end applications like automotive parts.

Particulate matter emissions from gasoline direct injection engines are a concern due to the health effects associated with ultrafine particles. This experimental study investigated sources of particulate matter emissions variability observed in previous tests and also examined the effect of ethanol content in gasoline on particle number (PN) concentrations and particle mass (PM) emissions. FTIR measurements of gas phase hydrocarbon emissions provided evidence that changes in fuel composition were responsible for the variability. Exhaust emissions of toluene and ethanol correlated positively with emitted PN concentrations, while emissions of isobutylene correlated negatively. Exhaust emissions of toluene and isobutylene were interpreted as markers of gasoline aromatic content and gasoline volatility respectively.

Adiabatic two-phase flow experiments have been carried out in an evaporator plate assembly which has entry and exit header vestibules on one side and a U pattern flow passage with round or cross ribbed protuberance in the channel. Over the practical flow range in common installation orientations, non-uniform distributions were found in both surface wetting on the internal walls of a single channel and the flow rates in a number of parallel channels. The poor performances of the plate surface wetting in single channel and the flow distribution in the multiple channels would severely limit the heat transfer capability of the current designs.

This paper presents an experimental study on the foaming behavior of recyclable high-melt-strength (HMS) branched polypropylene (PP) with CO2 as a blowing agent. The foamability of branched HMS PP has been evaluated using a tandem foaming extruder system. The effects of CO2 and nucleating agent contents on the final foam morphology have been thoroughly investigated. The low density (i.e., 12~14 fold), fine-celled (i.e., 107–109 cells/cm3) PP foams were successfully produced using a small amount of talc (i.e., 0.8 wt%) and 5 wt% CO2.

Determination of the solubility of a blowing agent, i.e. supercritical N2, in polypropylene (PP) and elastomer material is crucial for achieving high-quality thermoplastic polyolefin (TPO) foams in automotive industry. A magnetic suspension balance (MSB) was employed in the experiments to measure the apparent solubility, while the swollen volume predicted by the Sanchez-Lacombe (SL) equation of state (EOS) was used to account for the buoyancy effect. The volume swelling of the polymer/gas mixture and the gas solubilities for both PP and polyolefin elastomer were discussed.

Foaming of thermoplastic polyolefins (TPO) and thermoplastic elastomers (TPE) is gaining interest because of the lightweight and high performance to weight ratio of foamed automotive parts. Since foaming will occur mainly in the PP matrix in these PP-based automotive materials, understanding of the thermophysical properties of PP/gas mixtures is critically important. This paper will present a proposed methodology for measuring the swelling of polymer/gas mixtures. The preliminary experimental measurement of PP/N2 swelling at elevated temperatures and pressures will be discussed.

This paper demonstrates the effects of nano-clay on the microcellular foam processing of nylon. First, Nylon 6 nanocomposites with 1 wt% clay were prepared by a twin screw extruder. The nanocomposite structures were characterized by XRD and TEM. Nylon and its nanocomposites were foamed in extrusion using CO2. The cell morphologies of nylon and its nanocomposite foams were investigated. It appeared that the nano-clay not only enhanced cell nucleation, but also suppressed cell deterioration in the microcellular foaming of nylon.

Determination of the solubility of a blowing agent, i.e. supercritical CO2 or N2, in polypropylene (PP) is crucial for achieving high-quality PP and thermoplastic polyolefin (TPO) foams. A magnetic suspension balance (MSB) was employed in the experiments to measure the apparent solubility, while the swollen volume predicted by the Sanchez-Lacombe (SL) equation of state (EOS) and Simha-Somcynsky (SS) EOS was used to account for the buoyancy effect. The gas solubilities for both linear and branched PP were calculated and the effects of branching on the swollen volume and gas solubility were discussed.

The use of natural fibers for polymer composite materials has increased tremendously in the last few years. This type of reinforcements offers many advantages such as low density, low cost, high specific strength and low environmental impacts. The performance of the natural fiber composites are affected by the fiber loading, the individual mechanical properties of each component (fiber and matrix), and the fiber and matrix adhesion. Concerning the interfacial interaction, natural fibers present a major drawback because of poor compatibility of fibers with most hydrophobic thermoplastic and thermoset matrix. Hemp fiber/acrylic composites were manufactured with sheet molding technique recently. Although mechanical tests give promising results, they exhibit low tensile strength resulting from a poor fiber/matrix adhesion. The moisture resistance property of the sheet molded composites also needs further improvement.

Natural fiber reinforced polymer composites are beginning to find their way into the commercial automotive market. But, inadequate adhesion between hydrophilic natural fibers and hydrophobic matrix materials affects the performance of the resulting composites. In this study the effect of an environmental friendly fungal treatment on the adhesion characteristics of natural fibers is investigated. Firstly, changes in acid-base characteristics of the modified hemp fibers were studied using Inverse Gas Chromatography (IGC). Afterwards, composites were prepared using Resin Transfer Molding (RTM) process and the effect of modification on performance and durability of the composites was investigated.

The performance of low-adhesion surfaces in a realistic, in-flight icing environment with supercooled liquid droplets is evaluated using a NACA 0018 airfoil in the National Research Council of Canada Altitude Icing Wind Tunnel. This project was completed in collaboration with McGill University, the University of Toronto and the NRC Aerospace Manufacturing Technologies Centre in March 2022. Each collaborator used significantly different methods to produce low-adhesion surface treatments. The goal of the research program was to demonstrate if the low-adhesion surfaces reduced the energy required to de-ice or anti-ice an airfoil in an in-flight icing environment. Each collaborator had been developing their own low-adhesion surfaces, using bench tests in cold rooms and a spin rig in the wind tunnel to evaluate their performance. The most promising surface treatments were selected for testing on the airfoil.

A counter–flow propane/air diffusion flame (ϕ= 1.79) is used for a fundamental analysis of the effects of oxygenated additives on soot precursor formation. Experiments are conducted at atmospheric pressure using Gas Chromatography for gas sample analysis. The oxygenated additives dimethyl carbonate (DMC) and ethanol are added to the fuel keeping the total volumetric fuel flow rate constant. Results show 10 vol% DMC significantly reduces acetylene, benzene, and other flame pyrolysis products. Ethanol (10 vol%) shows, instead, more modest reductions. Peak acetylene and benzene levels decrease as the additive dosage increases for both DMC and ethanol. The additive's effect on the adiabatic flame temperature and the fuel stream carbon content does not correlate significantly with acetylene levels. However, there does appear to be a linear relationship between acetylene concentrations and both the additive's oxygen and C–C bond content.