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Composite materials are increasingly being used in the manufacturing of structural components in aeronautics industry. A consequent light-weight design of CFRP primary structures requires adhesive bonding as the optimum joining technique but is limited due to a lack of adequate quality assurance procedures. The successful implementation of a reliable quality assurance concept for adhesive bonding within manufacturing and in-service environments will provide the basis for increased use of lightweight composite materials for highly integrated aircraft structures thus minimizing rivet-based assembly. The expected weight saving for the fuselage airframe is remarkable and therefore the driver for research and development of key-enabling technologies. The performance of adhesive bonds mainly depends on the physico-chemical properties of adherend surfaces.