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Experimental study has been carried out on the effects of the micro-hole nozzle injector and ultra-high injection pressure on the mixture properties of D.I. Diesel engine. A manually operated piston screw pump, High Pressure Generator, was used to obtain ultra-high injection pressures. Three kinds of injection pressures, 100MPa, 200MPa, and 300MPa, were applied to a specially designed injector. Four kinds of nozzle hole diameters, 0.16mm, 0.14mm, 0.10mm, and 0.08mm, were adopted in this study. The laser absorption-scattering (LAS) technique was used to analyze the equivalence ratio distributions, Sauter mean diameter, spray tip penetration length, and other spray characteristics. The analyses of the experimental results show that the micro-hole nozzle and ultra-high injection pressure are effective to increase the turbulent mixing rate and to form the uniform and lean fuel-air mixture.