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In order to measure the droplets and vapor concentration inside a fuel spray, a dual-wavelength laser absorption-scattering technique was developed using the second harmonic (532nm) and the fourth harmonic (266nm) of a Nd:YAG laser and using dimethylnaphthalene as the test fuel. The investigation results show that dimethylnaphthalene, which has physical properties similar to diesel fuel, is almost transparent to visible light near 532nm and is a strong absorber of ultraviolet light near 266nm. Based on this result, the vapor concentration in a fuel spray can be determined by the two separate measurements: a transmission measurement at a non-absorbing wavelength to detect the droplets optical thickness and a transmission measurement at an absorbing wavelength to detect the joint vapor and droplets optical thickness. The droplets density can be determined by extinction imaging through the transmission at the non-absorbing wavelength.