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In this paper, characteristics of gas emission and particle size distribution are investigated in a common rail diesel engine fueled with biodiesel blends. Gas emission and particle size distribution are measured by AVL FTIR - SESAM and SMPS respectively. The results show that although biodiesel blends would result in higher NOx emissions, characteristics of NOx emissions were also dependent on the engine load for waste cooking oil methyl ester. Higher blend concentration results in higher NO2 emission after two diesel oxidation catalyst s (DOC). A higher blend concentration leads to lower CO and SO2 emissions. No significant difference of Alkene emission is found among biodiesel blends. The particle size distributions of diesel exhaust aerosol consist of a nucleation mode (NM) with a peak below 50N• m and an accumulation mode with a peak above 50N • m. B100 will result in lower particulates with the absence of NM.