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Flash boiling is considered a useful method in enhancing the liquid fuel jet break-up and spray atomization process for internal combustion engine applications. Spray atomization efficiency plays a vital role in the combustion process. Although some researches have demonstrated that flash boiling has the potential to improve the combustion efficiency and optimize emission-related issues, the effect of flash boiling spray characteristics on the combustion process has not been fully investigated. In this paper, spray characteristics and its related combustion process were studied via various non-intrusive diagnostics methods. The spray and combustion process under different test conditions were studied using an optical engine. It was found that by using flash boiling atomization, the combustion duration was reduced and IMEP enhanced significantly. Experimental results have built the relationship between flash boiling spray characteristics and the combustion performance in the engine.