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The effect of friction modifiers on the low-speed frictional properties of automatic transmission fluids (ATFs) was investigated by scanning force microscopy (SFM). A clutch lining material was covered by a droplet of test ATF, and a steel tip was scanned over the sample. The scanning speeds were varied from 0.13 to 8.56 mm /sec, and the frictional force was deduced from the torsion of the SFM cantilever. A reduction in dynamic friction due to the addition of the friction modifier was clearly observed over the entire speed range. This indicates that the boundary lubrication mechanism is dominant under this condition, and therefore surface-active friction modifiers can effectively improve the frictional characteristics. The friction reduction was more pronounced at lower sliding speeds. Thus addition of friction modifiers produced a more positive slope in the μ-ν (friction vs. sliding speed) plots, and would contribute to make wet clutch systems less susceptible to shudder vibrations.

The International Lubricant Standardization and Approval Committee (ILSAC) ATF subcommittee members have compared the two oxidation bench test methods, Aluminum Beaker Oxidation Test (ABOT) and Indiana Stirring Oxidation Stability Test (ISOT), using a number of factory-fill and service-fill ATFs obtained in Japan and in the US. In many cases, the ATFs were more severely oxidized after the ABOT procedure than after the same duration of the ISOT procedure. The relative severity of these two tests was influenced by the composition of the ATFs. The bench test oxidation data were compared with the transmission and the vehicle oxidation test data.

This paper describes the basic principles of extensional rheometry, and the successful application to a variety of automotive fluids, including gear lubricants, paints, and forming lubricants. These fluids are used under very complex flow fields containing strong extensional (elongational) components. While exact derivation of extensional viscosities involves sophisticated theories, the measurement of liquid filament break-up time can provide fruitful information. Gear lubes showed different break-up time according to the kinematic viscosities. Addition of viscosity modifier (acrylic copolymer) significantly increased the breakup time, whereas surfactants had little effect. Clearcoat paint sample increased the breakup time, perhaps due to the deterioration. The waxy stamping lubricant showed remarkable change in the extensional properties as the temperature is raised.