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Technical Paper

Physical Characterization of Biodiesel Particle Emission by Electron Microscopy

2013-10-15
2013-32-9150
Nanostructures of diesel and biodiesel engine particulate matters (PMs) were investigated by using a Transmission Electron Microscopy (TEM). The average single particle sizes of biodiesel and diesel PMs are approximately 30-40 nm and 50-60 nm, respectively. Image processing process was used to estimate each carbon platelet length by using TEM image. The average carbon platelet length of biodiesel and diesel PMs are in the range of 0.1-7.0 nm. Moreover, carbon atoms per cubic volume of PMs are approximately 500-900. The result shows that engine load and fuel property are strongly impact on the size of single particle and carbon atom density of particle. This is one of interesting behaviors need to be investigated for better understanding. The results of this research would be used as basic information for design and develop removing process of PM emitted from engine combustion which using in diesel and biodiesel fuels.
Technical Paper

Impact of TiO2 and V2O5 on Sintered Mullite Porous Microstructure and Soot Oxidation Kinetics Using SEM and TGA

2019-03-25
2019-01-1407
The exhaust emissions from diesel combustion are the sources of particulate matter emitted to the atmosphere, which are components of air pollution that implicated in human health such as lung cancer. At present the diesel particulate filter can remove PM from the exhaust gas before emitted to the atmosphere. This research is investigating morphology and structure of acicular mullite to develop the fabrication process filter in order to study particulate matters trapping and oxidation mechanisms. This paper used two main substances to study the structure of diesel particulate filter (DPFs); Aluminum oxide (Al2O3) and Silicon dioxide (SiO2). These are mainly in the conventional DPFs. The variable substances are Titanium dioxide (TiO2) and Vanadium oxide (V2O5), which added to investigate and produce the acicular mullite DPFs structure. The mullite samples were sintered at 1300 oC with holding time of 1 h.
Technical Paper

Impact of Engine Oil Additives on Nanostructure and Oxidation Kinetics of Diesel and Synthetic Biodiesel Particulate Matters using Electron Microscopy

2019-12-19
2019-01-2351
Physicochemical characteristics of particulate matters which are influenced by engine oil additives from engine combustion of diesel and synthetic biodiesel: hydrotreated vegetable oil (HVO) were successfully investigated using electron microscopy, electron dispersive x-ray spectroscopy and thermogravimetric analysis. The agglomerate structure of diesel PM, HVO PM and diesel blending lubricant PM are similar in micro-scales. However, nanostructure of soot is a spherical shape composed of curve line crystallites while the metal oxide ash nanostructure is composed of parallel straight line hatch patterns. The oxidation kinetics of fuel blending lubricant PMs are higher than neat fuel PMs due to catalytic effect of incombustible metal additives from engine lubricating oil.
Technical Paper

Impact of Biodiesel on Small CI Engine Combustion Behavior and Particle Emission Characteristic

2017-11-05
2017-32-0094
Diesel engines are high thermal efficiency because of high compression ratio but produce high concentration of particulate matter (PM) because of direct injection fuel diffusion combustion. PM must be removed from the exhaust gas to protect human health. This research describes biodiesel engine performance, efficiency and combustion behavior using combustion pressure analyzer. It was clearly observed that PM emitted from CI engines can be reduced by using renewable bio-oxygenated fuels. The morphology and nanostructure of fossil fuel and biofuel PMs were investigated by using a Scanning electron microscopy (SEM) and Transmission electron microscopy (TEM). The morphology of biodiesel and diesel doesn’t have much different in the viewpoint of particulate matter trapping using DPF micro surface pores. The agglomerated ultrafine particles and primary nanoparticles sizes of diesel and biodiesel engine’s PM are approximately 50-500 nm and 20-50 nm, respectively.
Technical Paper

Effect of Biofuel and Soot on Metal Wear Characteristic Using Electron Microscopy and 3D Image Processing

2017-11-05
2017-32-0095
The soot contamination in used engine oils of diesel engine vehicles was about 1% by weight. The soot and metal wear particle sizes might be in the range of 0-1 µm and 1-25 µm, respectively. The characteristics of soot affecting on metal wear was investigated. Soot particle contamination in diesel engine oil was simulated using carbon black. Micro-nanostructure of soot particles were studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and laser diffraction spectroscopy (LDS). The metal wear behavior was studied by means of a Four-Ball tribology test with wear measured. Wear roughness in micro-scale was investigated by high resolution optical microscopy (OM) , 3D rendering optical technique and SEM image processing method. It was found that the ball wear scar diameter increased proportionally to the soot primary particle size. The effect of biodiesel contamination were also increasing in wear scar diameter.
Technical Paper

Characterization of Carbon Fiber and Glass Fiber’s Micro and Nanostructure Using Electron Microscopy, Raman Spectroscopy and XRD Analysis

2019-03-25
2019-01-1441
Nowadays, most manufacturers are looking for the improvement of lightweight parts and other components in the automobile field. Carbon fiber and glass fiber are the most effective materials for their requirement to reduce the weight in vehicles due to their light weight and high tensile strength. The diameter of carbon fiber is 6 μm while glass fiber diameter is 17 μm. The mechanical tensile force of carbon fiber and glass fiber are 430 N and 290 N respectively on fiber alone without matrix. Carbon fibers are gradually smaller in each filament due to tensile force. Approximately 5 mm are elongated for both carbon fiber and glass fiber in tensile test report. In current research, characteristic and tensile force of carbon fiber and glass fiber were investigated by using electron microscopy, Raman spectroscopy and XRD.
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