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An experimental study on emission formation processes, such as these of nitric oxide, particulate and total hydrocarbon in a small direct injection (D.I.) diesel engine was carried out by using a newly developed total in-cylinder sampling technique. The sampling method consisted of rapidly opening a blowdown valve attached to the bottom of the piston bowl, and quickly transferring most of the in-cylinder contents into a large sampling chamber below the piston. No modification of the intake and exhaust ports in a cylinder head was required for the installation of the blowdown apparatus. The sampling experiment gave a history of spatially-averaged emission concentrations in the cylinder. The effects of several engine variables, such as the length-to-diameter ratio of the nozzle hole, the ratio of the piston bowl diameter to the cylinder bore and the intake swirl ratio, on the emission formation processes were investigated.