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Plug-in hybrid electric vehicles (PHVs) consume both fossil fuel and grid electricity, which imposes emission testing challenges on the current constant volume sampler (CVS) test method. One reason is that in the charge-depleting cycle, PHVs having all-electric range operate the engine for a small portion of the traction energy need, causing the CVS to overdilute the exhaust gas. The other reason is that the dilution factor (DF) in the EPA calculation has an error caused by ignoring the CO₂ concentration in ambient air. This paper evaluates these challenges by testing a Toyota PHV on the industry standard CVS system combined with additional continuous sampling methodology for continuous diluents, smooth approach orifice (SAO) measurement for ambient air flow, and fuel flow meter (FFM) measurement for fuel consumption. The current EPA DF can produce an error resulting in higher mass calculation.