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A quantitative and time-resolved technique has been developed to probe the fuel distribution very near the nozzle of a high-pressure diesel injector. This technique uses the absorption of synchrotron x-rays to measure the fuel mass with good time and position resolution. The penetrating power of x-rays allows measurements that are difficult with other techniques, such as quantitative measurements of the mass and penetration measurements of the trailing edge of the spray. Line-of-sight measurements were used to determine the fuel density as a function of time. The high time resolution and quantitative nature of the measurement also permit an accurate measure of the instantaneous mass flow rate through the nozzle.