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Ash accumulation in the channels of ceramic, honeycomb-type particulate filters is controlled by several key parameters, which are the focus of this study. Ultimately, it is the formation of ash deposits, their transport, and the manner in which the ash accumulates in the particulate filter, which determines the useful service life of the filter and its resulting impact on engine performance. Although significant variations in ash deposit properties and their spatial distribution within the filter channels have been reported, depending on the filter's application, understanding the key parameters and mechanisms, such as the effects of exhaust flow and temperature conditions, as well as the processes occurring during filter regeneration events (whether passive or active) are critical in developing improved filter ash management strategies.

Ash inside a honeycomb-configured diesel particulate filter (DPF) inlet channel accumulates both as a cake layer along the channel walls and as a “plug” towards the back of the channel. Experimental studies of DPF ash distribution have shown both an axial variation of deposits along channels and accumulation towards the end plugs. This study evaluates the sensitivity of DPF pressure drop on ash axial distribution and the potential to reduce flow restrictions by controlling and optimizing the spatial distribution of ash inside DPF channels. A computational model has been used in conjunction with experimental data to illustrate the sensitivity of ash spatial distribution on DPF performance. The classical constant-thickness DPF one-dimensional models have substantially been updated to include layer thickness axial variations. Material properties, such as ash characteristics, are provided by recent experiments at the authors' laboratory.

The accumulation of soot and lubrication-derived ash particles in a diesel particulate filter (DPF) increases exhaust flow restriction and negatively impacts engine efficiency. Previous studies have described the macroscopic phenomenon and general effects of soot and ash accumulation on filter pressure drop. In order to enhance the fundamental understanding, this study utilized a novel apparatus that of a dual beam scanning electron microscope (SEM) and focused ion beam (FIB), to investigate microscopic details of soot and ash accumulation in the DPF. Specifically, FIB provides a minimally invasive technique to analyze the interactions between the soot, ash, catalyst/washcoat, and DPF substrate with a high degree of measurement resolution. The FIB utilizes a gallium liquid metal ion source which produces Ga+ ions of sufficient momentum to directionally mill away material from the soot, ash, and substrate layers on a nm-μm scale.

Current CJ-4 lubricant specifications place chemical limits on diesel engine oil formulations to minimize the accumulation of lubricant-derived ash in diesel particulate filters (DPF). While lubricant additive chemistry plays a strong role in determining the amount and type of ash accumulated in the DPF, a number of additional factors play important roles as well. Relative to soot particles, whose residence time in the DPF is short-lived, ash particles remain in the filter for a significant fraction of the filter's useful life. While it is well-known that the properties (packing density, porosity, permeability) of soot deposits are primarily controlled by the local exhaust conditions at the time of particle deposition in the DPF, the cumulative operating history of the filter plays a much stronger role in controlling the properties and distribution of the accumulated ash.

Radio frequency (RF)-based sensors provide a direct measure of the particulate filter loading state. In contrast to particulate matter (PM) sensors, which monitor the concentration of PM in the exhaust gas stream for on-board diagnostics purposes, RF sensors have historically been applied to monitor and control the particulate filter regeneration process. This work developed an RF-based particulate filter control system utilizing both conventional and fast response RF sensors, and evaluated the feasibility of applying fast-response RF sensors to provide a real-time measurement of engine-out PM emissions. Testing with a light-duty diesel engine equipped with fast response RF sensors investigated the potential to utilize the particulate filter itself as an engine-out soot sensor.

Diesel Particulate Filters (DPF) are a key component in many on- and off-road aftertreatment systems to meet increasingly stringent particle emissions limits. Efficient thermal management and regeneration control is critical for reliable and cost-effective operation of the combined engine and aftertreatment system. Conventional DPF control systems predominantly rely on a combination of filter pressure drop measurements and predictive models to indirectly estimate the soot loading state of the filter. Over time, the build-up of incombustible ash, primarily derived from metal-containing lubricant additives, accumulates in the filter to levels far exceeding the DPF's soot storage limit. The combined effects of soot and ash build-up dynamically impact the filter's pressure drop response, service life, and fuel consumption, and must be accurately accounted for in order to optimize engine and aftertreatment system performance.

Efficient aftertreatment management requires accurate sensing of both particulate filter soot and ash levels for optimized feedback control. Currently a combination of pressure drop measurements and predictive models are used to indirectly estimate the loading state of the filter. Accurate determination of filter soot loading levels is challenging under certain operating conditions, particularly following partial regeneration events and at low flow rate (idle) conditions. This work applied radio frequency (RF)-based sensors to provide a direct measure of the particulate filter soot levels in situ. Direct measurements of the filter loading state enable advanced feedback controls to optimize the combined engine and aftertreatment system for improved DPF management. This study instrumented several cordierite and aluminum titanate diesel particulate filters with RF sensors. The systems were tested on a range of light- and heavy-duty applications, which included on- and off-road engines.

The increasing use of diesel and gasoline particulate filters requires advanced on-board diagnostics (OBD) to prevent and detect filter failures and malfunctions. Early detection of upstream (engine-out) malfunctions is paramount to preventing irreversible damage to downstream aftertreatment system components. Such early detection can mitigate the failure of the particulate filter resulting in the escape of emissions exceeding permissible limits and extend the component life. However, despite best efforts at early detection and filter failure prevention, the OBD system must also be able to detect filter failures when they occur. In this study, radio frequency (RF) sensors were used to directly monitor the particulate filter state of health for both gasoline particulate filter (GPF) and diesel particulate filter (DPF) applications.

Sintered metal fiber (SMF) diesel particulate filters (DPF) has more than one order of magnitude lower pressure drop compared to a granular or reaction-born DPF of the same (clean) filtration efficiency. To better understand the filtration process and optimize the filter performance, metal fiber filter models are developed in this study. The major previous theoretical models for clean fibrous filter are summarized and compared with experimental data. Furthermore, a metal fiber DPF soot loading model, using similar concept developed in high efficiency particulate air (HEPA) filter modeling, is built to simulate filter soot loading performance. Compared with experimental results, the soot loading model has relatively good predictions of filter pressure drop and filtration efficiency.

The increasing use of gasoline direct injection (GDI) engines coupled with the implementation of new particulate matter (PM) and particle number (PN) emissions regulations requires new emissions control strategies. Gasoline particulate filters (GPFs) present one approach to reduce particle emissions. Although primarily composed of combustible material which may be removed through oxidation, particle also contains incombustible components or ash. Over the service life of the filter the accumulation of ash causes an increase in exhaust backpressure, and limits the useful life of the GPF. This study utilized an accelerated aging system to generate elevated ash levels by injecting lubricant oil with the gasoline fuel into a burner system. GPFs were aged to a series of levels representing filter life up to 150,000 miles (240,000 km). The impact of ash on the filter pressure drop and on its sensitivity to soot accumulation was investigated at specific ash levels.

Accurate knowledge of diesel particulate filter (DPF) particulate matter (PM) loading is critical for robust and efficient operation of the combined engine-exhaust aftertreatment system. Furthermore, upcoming on-board diagnostics regulations require on-board technologies to evaluate the status of the DPF. This work describes the application of radio frequency (RF) - based sensing techniques to accurately measure DPF particulate matter levels. A 1.9L GM turbo diesel engine and a DPF with an RF-sensor were studied. Direct comparisons between the RF measurement and conventional pressure-based methods were made. Further analysis of the particulate matter loading rates was obtained with a mass-based total PM emission measurement instrument (TEOM) and DPF gravimetric measurements.

Diesel particulate filters (DPF) are a common component in emission-control systems of modern clean diesel vehicles. Several DPF materials have been used in various applications. Silicone Carbide (SiC) is common for passenger vehicles because of its thermal robustness derived from its high specific gravity and heat conductivity. However, a segmented structure is required to relieve thermal stress due to SiC's higher coefficient of thermal expansion (CTE). Cordierite (Cd) is a popular material for heavy-duty vehicles. Cordierite which has less mass per given volume, exhibits superior light-off performance, and is also adequate for use in larger monolith structures, due to its lower CTE. SiC and cordierite are recognized as the most prevalent DPF materials since the 2000's. The DPF traps not only combustible particles (soot) but also incombustible ash. Ash accumulates in the DPF and remains in the filter until being physically removed.

The formation and transport processes governing the build-up of incombustible ash deposits in diesel particulate filters (DPF) are influenced to a large extent by the filter's operating history. More specifically, the regeneration process, whether active, passive, or some variation of the two, has long been assumed to exert significant influence on the resulting ash characteristics. Until recently, only limited circumstantial evidence was available to describe differences in ash properties and distribution impacting DPF performance for filters subjected to different regeneration strategies. This work presents, for the first time, results from a comprehensive series of evaluations with optically-accessible DPF core samples showing the processes controlling the formation, transport, and interaction of the soot and ash deposits over a range of DPF regeneration conditions.

The use of biodiesel and its blends with ultra low sulfur diesel (ULSD) is gaining significant importance due to its ability to burn in conventional diesel engines with minor modifications. However the chemical and physical properties of biodiesel are different compared to the conventional ULSD. These differences directly impact the injection, spray formation, auto ignition and combustion processes which in turn affect the engine-out emissions. To understand the effect of fueling with B-20, tests were conducted on a single cylinder 0.42L direct injection research diesel engine. The engine is equipped with a common rail injection system, variable EGR and swirl control systems and was operated at a constant engine speed of 1500 rpm and 3 bar IMEP to simulated turbocharged conditions. Injection timing and duration were adjusted with B-20 at different locations of peak premixed combustions (LPPC) and two different swirl ratios to achieve 3 bar IMEP.

Inorganic engine lubricant additives, which have various specific, necessary functions such as anti-wear, leave the combustion chamber bound to soot particles (approximately ≤1% by mass) as ash [13], and accumulate in aftertreatment components. The diesel particulate filter (DPF) is especially susceptible to ash-related issues due to its wall-flow architecture which physically traps most of the soot and ash emissions. Accumulated lubricant-derived ash results in numerous problems including increased filter pressure drop and decreased catalytic functionality. While much progress has been made to understand the macroscopic details and effects of ash accumulation on DPF performance, this study explores the nano- and micron-scale forces which impact particle adhesion and mobility within the particulate filter.

Reducing cold-start emissions to meet increasingly stringent emissions limits requires fast activation of exhaust system sensors and aftertreatment control strategies. One factor delaying the activation time of current exhaust sensors, such as NOx and particulate matter (PM) sensors, is the need to protect these sensors from water present in the exhaust system. Exposure of the ceramic sensing element to water droplets can lead to thermal shock and failure of the sensor. In order to prevent such failures, various algorithms are employed to estimate the dew point of the exhaust gas and determine when the exhaust system is sufficiently dry to enable safe sensor operation. In contrast to these indirect, model-based approaches, this study utilized radio frequency (RF) sensors typically applied to monitor soot loading levels in diesel and gasoline particulate filters, to provide a direct measurement of stored water levels on the ceramic filter elements themselves.

The Cu-zeolite (CuZ) SCR catalyst enables higher NOx conversion efficiency in part because it can store a significant amount of NH3. “NH3 storage control”, where diesel exhaust fluid (DEF) is dosed in accord with a target NH3 loading, is widely used with CuZ catalysts to achieve very high efficiency. The NH3 loading actually achieved on the catalyst is currently estimated through a stoichiometric calculation. With future high-capacity CuZ catalyst designs, it is likely that the accuracy of this NH3 loading estimate will become limiting for NOx conversion efficiency. Therefore, a direct measurement of NH3 loading is needed; RF sensing enables this. Relative to RF sensing of soot in a DPF (which is in commercial production), RF sensing of NH3 adsorbed on CuZ is more challenging. Therefore, more attention must be paid to the “microwave resonance cavity” created within the SCR assembly. The objective of this study was to develop design guidelines to enable and enhance RF sensing.

Reliable means for on-board detection of particulate filter failures or malfunctions are needed to meet diagnostics (OBD) requirements. Detecting these failures, which result in tailpipe particulate matter (PM) emissions exceeding the OBD limit, over all operating conditions is challenging. Current approaches employ differential pressure sensors and downstream PM sensors, in combination with particulate filter and engine-out soot models. These conventional monitors typically operate over narrowly-defined time windows and do not provide a direct measure of the filter’s state of health. In contrast, radio frequency (RF) sensors, which transmit a wireless signal through the filter substrate provide a direct means for interrogating the condition of the filter itself.

Ash accumulation in diesel particulate filters, mostly from essential lubricant additives, decreases the filter's soot storage capacity, adversely affects fuel economy, and negatively impacts the filter's service life. While the adverse effects of ash accumulation on DPF performance are well known, the underlying mechanisms controlling these effects are not. To address these issues, results of detailed measurements with specially formulated lubricants, correlating ash properties to individual lubricant additives and their effects on DPF pressure drop, are presented. Investigations using the specially-formulated lubricants showed ash consisting primarily of calcium sulfates to exhibit significantly increased flow resistance as opposed to ash primarily composed of zinc phosphates. Furthermore, ash accumulated along the filer walls was found to be packed approximately 25% denser than ash accumulated in the channel end-plugs.

Ash, mostly from essential lubricant additives, affects diesel particulate filter (DPF) pressure-drop sensitivity and limits filter service life. It raises concern in the lubricant industry to properly specify new oils, and engine and aftertreatment system manufacturers have attempted to find ways to mitigate the problem. To address these issues, results of detailed measurements of ash characteristics in the DPF and their effects on filter performance are presented. In this study, a heavy-duty diesel engine was outfitted with a specially designed rapid lubricant degradation and aftertreatment ash loading system. Unlike previous studies, this system allows for the control of specific exhaust characteristics including ash emission rate, ash-to-particle ratio, ash composition, and exhaust temperature and flow rates independent of the engine operating condition.