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In this paper an estimation method on location of peak pressure (LPP) employing flame ionization measurement, with the spark plug as a sensor, was discussed to achieve combustion parameters estimation at quick start of HEV engines. Through the cycle-based ion signal analysis, the location of peak pressure can be extracted in individual cylinder for the optimization of engine quick start control of HEV engine. A series of quick start processes with different cranking speed and engine coolant temperature are tested for establishing the relationship between the ion signals and the combustion parameters. An Artificial Neural Network (ANN) algorithm is used in this study for estimating these two combustion parameters. The experiment results show that the location of peak pressure can be well established by this method.