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A miniature quadrupole mass spectrometer array and gas chromatograph have been designed and built for NASA flight missions. Without the gas chromatograph the mass spectrometer is to be used for detection, by astronauts in EVA, of N2, O2, the hydrazines, and NH3 leaks in the hull of the International Space Station, and of adsorbed hydrazines on the astronauts’ suits. The fully-adapted astronaut system, with all software and visual readout, is called the Trace Gas Analyzer. When interfaced with the miniature gas chromatographic system, the mass spectrometer will be useful for a variety of NASA missions involving more complex gas mixtures. The missions include planetary exploration (to Venus, Europa, Titan, etc.), as well as cabin-air monitoring for long-duration human flight to the Moon, Mars, and beyond.

Bacillus sp. ATCC 29669 was isolated from microbial fallout in clean rooms during the assembly of the Viking Spacecraft missions to Mars, making it a potential contamination concern for outbound space missions. Spores from this bacterial strain were found to be thirty times more resistant to dry heat than B. atrophaeus. Spore inactivation rates under vacuum controlled humidity were faster than rates obtained under ambient humidity. Inactivation rates for these heat resistant spores are important considerations for planetary protection implementation where temperature, time and humidity conditions are used to estimate the effectiveness of dry heat microbial reduction (DHMR) procedures.

Various candidates for nonpetroleum electric and hybrid vehicle (EHV) subsystems have been evaluated as part of the Advanced Vehicle (AV) Assessment at the Jet Propulsion Laboratory. The subsystems include battery and power-peaking energy storage, heat engine and fuel cell energy conversion devices, motor/controller subsystems, transmissions, and vehicle subsystem (structure and body) technologies. The primary objective of this effort, was to project the mature capabilities of the various components in the 1990’s for application in the systems evaluations in the next phase of this activity. This paper presents the basic characteristics of the subsystems and compares their capabilities with projected AV subsystem requirements.

This paper describes a study on the capillary limit of a loop heat pipe (LHP) with two evaporators and two condensers. Both theoretical analysis and experimental investigation are performed. Experimental tests conducted include heat load to one evaporator only, even heat loads to both evaporators, and uneven heat loads to both evaporators. Test results show that after the capillary limit is exceeded, vapor will penetrate through the wick of the weaker evaporator, and the compensation chamber (CC) of that evaporator will control the loop operating temperature regardless of which CC has been in control prior to the event. Because the evaporator can tolerate vapor bubbles, the loop can continue to work after vapor penetration. As the loop operating temperature increases, the system pressure drop actually decreases due to a decrease in liquid and vapor viscosities. Thus, the loop may reach a new steady state at a higher operating temperature after vapor penetration.

In support of the National Aeronautics and Space Administration(NASA), a laboratory has been established at the Jet Propulsion Laboratory (JPL) to evaluate the characteristics of chemical sensors which are candidates for use in a controlled chemical processing life support system. Such a facility is required for characterizing those sensors under development as well as those commercially available but whose functional properties are typically based upon operating in industrial environments that will not be completely synonomous with space operations. Space environments, such as an orbiting station or lunar base, will generally have different sensor requirements than terrestrial applications with respect to size, multifunctionality, sensitivity, reliability, temperature, ruggedness, mass, consumables, life, and power requirements. Both commercially available and developmental moisture sensors have been evaluated.

NASA's proposed lunar lander, Altair, will be exposed to vastly different external temperatures following launch till its final destination on the moon. In addition, the heat rejection is lowest at the lowest environmental temperatures (0.5 kW @ 4K) and highest at the highest environmental temperature (4.5 kW @ 215K). This places a severe demand on the radiator design to handle these extreme turn-down requirements. A radiator with digital turn-down capability is currently under study at JPL as a robust means to meet the heat rejection demands and provide freeze protection while minimizing mass and power consumption. Turndown is achieved by independent control of flow branches with isolating latch valves and a gear pump to evacuate the isolated branches. A bench-top test was conducted to characterize the digital radiator concept. Testing focused on the demonstration of proper valve sequencing to achieve turn-down and recharge of flow legs.

The Mars Exploration Rover (MER) flight system uses mechanical, paraffin-actuated heat switches as part of its secondary battery thermal control system. This paper describes the design, flight qualification, and performance of the heat switch. Although based on previous designs by Starsys Research Corporation1,2, the MER mission requirements have necessitated new design features and an extensive qualification program. The design utilizes the work created by the expansion of a paraffin wax by bringing into contact two aluminum surfaces, thereby forming a heat conduction path. As the paraffin freezes and contracts, compression springs separate the surfaces to remove the conduction path. The flight qualification program involved extensive thermal performance, structural, and life testing.

A paraffin-actuated heat switch has been developed for thermal control of the batteries used on the 2003 Mars Exploration Rovers. The heat switch is used to reject heat from the rover battery to a radiator. This paper describes the development test program designed, in part, to measure the thermal conductance of the heat switch in an 8 Torr CO2 environment over the expected operating temperature range of the battery. The switch has a closed conductance of about 0.6 W/°C and an open conductance of 0.019 W/°C. The test program also included measuring the battery temperature profile over a hot case and a cold case Mars diurnal cycle. The test results confirm that the battery will remain well within the upper and lower allowable flight temperatures in both cases.

Passively activated thermal control valves were developed for use in a mechanically pumped single-phase fluid liquid loop (MPFL) of the Mars Science Laboratory (MSL) rover. A key approach to the thermal control of the rover with the fluid loop is to control the flow through the rover's heat generating or heat rejecting components. This is achieved by either splitting or mixing the fluid stream coming from different branches of the system at different temperatures; actively or passively controlled flow valves are typically used for such purposes. To meet the thermal control requirements of the Mars Science Laboratory (MSL) rover, a splitting and a mixing thermal control valves with gradual control capabilities using a linear thermal actuator and a spool was developed at Jet Propulsion Laboratory (JPL). The key feature of these control valves is the balancing of the flow through the various branches of the fluid loop in order to balance the heat loads of the whole thermal system.

The recent development of single-mode continuous wave distributed feedback mid-IR interband cascade lasers operating at thermoelectric cooler temperatures is presented. Also, latest progress of interband cascade lasers is reported.

In order to meet microbial reduction requirements for all Mars in-situ life detection and sample return missions, entire planetary spacecraft (including planetary entry probes and planetary landing capsules) may have to be exposed to a qualified sterilization process. At JPL, we are developing a low temperature (~45°C) vapor phase hydrogen peroxide sterilization process. This process is currently being used by the medical industry and its effectiveness is well established. In order to effectively and safely apply this technology to sterilize a spacecraft, which is made out of various man-made materials and electronic circuit boards, the following technical issues need to be resolved: 1. Efficacy of sterilization process. 2. Diffusion of H2O2 under sterilization process conditions into hard to reach places. 3. Materials and components compatibility with the sterilization process. 4. Development of methodology to protect (isolate) sensitive components (i.e. electronic ) from H2O2 vapor.

The Orbiting Carbon Observatory (OCO) will carry a single science instrument scheduled for launch on an Orbital Sciences Corporation LeoStar-2 architecture spacecraft bus in December 2008. The science objective of the OCO instrument is to collect spaced-based measurements of atmospheric CO2 with the precision, resolution, and coverage needed to identify CO2 sources and sinks and quantify their seasonal variability. The instrument will permit the collection of spatially resolved, high resolution spectroscopic observations of CO2 and O2 absorption in reflected sunlight over both continents and oceans. These measurements will improve our ability to forecast CO2 induced climate change. The instrument consists of three bore-sighted, high resolution grating spectrometers sharing a common telescope with similar optics and electronics.

Phoenix is NASA's first Mars Scouts Mission that will place a soft-lander on the Martian surface at a high northern latitude. Much of the Mars surface environmental flight data from landed missions pertains to the near-equatorial regions. However, orbital observations have yielded very useful data about the surface environment. These data along with a simple, but highly effective one-dimensional atmospheric model was used to develop the Phoenix surface thermal environment. As candidate landing sites were identified, parametric studies including statistical variations were conducted to prescribe minimum nighttime and maximum daytime temperature design Sols (a Martian day). Atmospheric effects such as clouds and ice were considered. Finally, recent candidate landing site imaging conducted by the Mars Reconnaissance Orbiter revealed that the prime site contained a much higher rock density than first thought.

The capabilities of the JPL Electronic Nose have been expanded to include characteristics required for a Technology Demonstration schedule on the International Space Station (ISS) in 2008-2009 [1,2]. Concurrently, to accommodate specific needs on ISS, the processes, tools and analyses which influence all aspects of development of the device have also been expanded. The Third Generation ENose developed for this program uses two types of sensor substrates, newly developed inorganic and organic sensor materials, redesigned electronics, onboard near real-time data analysis and power and data interfaces specifically for ISS. This paper will discuss the Third Generation ENose with a focus on detection of mercury in the parts-per-billion range.

This study of samples collected from Mars 01 Orbiter was conducted to gain a better understanding and practical experience in methods to process and preserve samples intended for planetary protection analysis. Samples were evaluated for the viable growth of microbes, the molecular biomarker adenosine triphosphate (ATP), and the presence of lipopolysaccharide, a bacterial cell wall component. Losses were observed in the number of viable microbes after freezing as well as in the detectable lipopolysaccharide. Two independent studies of pooled cleanroom samples demonstrate good ATP recovery and consistent values after freezing at −20 °C.

An array-based sensing system based on 32 polymer/carbon composite conductometric sensors is under development at JPL. Until the present phase of development, the analyte set has focused on organic compounds (common solvents) and a few selected inorganic compounds, notably ammonia and hydrazine. The present phase of JPL ENose development has added two inorganics to the analyte set: mercury and sulfur dioxide. Through models of sensor-analyte response developed under this program coupled with a literature survey, approaches to including these analytes in the ENose target set have been determined.

An array-based sensing system based on polymer-carbon composite conductometric sensors is under development at JPL for use as an environmental monitor in the International Space Station. Sulfur dioxide has been added to the analyte set for this phase of development. Using molecular modeling techniques, the interaction energy between SO2 and polymer functional groups has been calculated, and polymers selected as potential SO2 sensors. Experiment has validated the model and two selected polymers have been shown to be promising materials for SO2 detection.

Dry heat microbial reduction is an approved method to reduce the microbial bioburden on space-flight hardware prior to launch to meet flight project planetary protection requirements. Microbial bioburden reduction also occurs if a spacecraft enters a planetary atmosphere (e.g., Mars) and is heated by frictional forces. However, without further studies, administrative credit for this reduction cannot be applied. The killing of Bacillus subtilis var. niger spores has been examined and lethality data has been collected by placing spores in a vacuum oven or thermal spore exposure vessels (TSEV) in a constant temperature bath. Using this lethality data, a preliminary mathematical model is being developed that can be used to predict spore killing at different temperatures. This paper will present the lethality data that has been collected at this time and the planned future studies.

The development of tunable diode laser systems in the 2 - 5 μm spectral region will have numerous applications for trace gas detection. To date, the development of such systems has been hampered by the difficulties of epitaxial growth, and device processing in the case of the Sb-based materials system. One of the compounding factors in this materials system is the use of aluminum containing compounds in the laser diode cladding layers. This makes the regrowth steps used in traditional lasers very difficult. As an alternative approach we are developing laterally coupled antimonide based lasers structures that do not require the regrowth steps. In this paper, the materials growth, device processing and development of the necessary drive electronics for an antimony based tunable diode laser system are discussed.

The Third Generation ENose is an air quality monitor designed to operate in the environment of the US Lab on the International Space Station. It detects a selected group of analytes at target concentrations in the ppm regime at an environmental temperature range of 18 - 30 °C, relative humidity from 25 - 75% and pressure from 530 to 760 torr. The abilities of the device to detect ten analytes, to reject confounders as “unknown” and to deconvolute mixtures of two analytes under varying environmental conditions has been tested extensively in the laboratory. Results of ground testing showed an overall success rate for detection, identification and quantification of analytes of 87% under nominal temperature and humidity conditions and 83% over all conditions.