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A pancake-type constant-volume combustion chamber was used to investigate the combustion and NOx emission characteristics of propane-air and hydrogen-air mixtures under various charge stratification patterns, which were obtained by variations of the initial charge and injected mixture concentrations and the ignition spark timing. A planar laser-induced fluorescence from nitrogen dioxide as gas fuel tracer was applied to measure the mixture distribution in the test chamber. The second harmonic output of pulsed Nd; YAG laser was used as a light source for fluorescence excitation. The fluorescence images were corrected by a gated image-intensified CCD camera. The quantitative analysis of fuel concentration was made possible by the application of linearity between fluorescence intensity and NO2 concentration at low trace level.