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This paper provides an insight into the design of a compound combustion chamber, with square and circular cavities, for use in a direct-injection diesel engine. Automotive diesel engines using square combustion chamber design have shown improvement in oxides of nitrogen and particulate exhaust emissions. In spite of this, neither the quality of mixture formation in such chambers nor the relationship between the engine performance and combustion chamber designs have been adequately addressed. Compound combustion chambers have potential to combine attributes of square and circular chambers to provide improved engine performance. An experimental study, based on liquid injection technique (LIT), was conducted to evaluate mixture formation in compound combustion chambers of different designs. These chambers have square geometry of depth "h" at the top and a curricular cavity at the bottom, with the total chamber depth being "H."