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A Mg-5.0wt.%Al-2.0wt.%Ca alloy (AC52) was cast at different cooling rates varying from 0.5 to 65 °C/s. The dendrites was characterized by determining the secondary dendrite arm spacing (SDAS) and the volume fraction of secondary eutectic phases with the linear intercept and point counting methods, respectively. The SDAS decreases significantly with increasing cooling rates, while the volume fraction of the eutectic phase increases from 10.8 ± 1.44 vol.% at 0.5 °C/s to 20.4 ± 1.52 vol.% at 20 °C/s. However, a further increase in cooling rate beyond 20 °C/s has limited influence on the volume fraction of eutectic phases. A large number of dispersed eutectic phases were observed in the primary α-Mg of the alloys cast at low cooling rates. Although, at the microscale, there were no dispersed eutectic phases in alloys cast at a high cooling rate of 30 °C/s, nanoscale eutectic phases were found by TEM observation.