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The effect of wall temperature on single surface flame quenching and flame structure of an atmospheric premixed methane-air flame was studied. The luminous region of a laminar flame was located at an angle of 45 degrees to a temperature- controlled surface. C2 laser-induced fluorescence was used as an indicator of flame position while Raman spectroscopy was used to determine gas temperature profiles near the surface. These measurements were conducted for wall positions (vertical distance from the surface) ranging from 50 mm to 1.0 mm and wall temperatures ranging from 150 °C to 600 °C. C2 laser-induced fluorescence measurements indicated flame position is affected by the presence of a surface and the surface temperature. Larger C2 fluorescence intensity values were observed for higher wall temperatures at all distances from the surface.